CARBANILIC ACID, p-BROMODITHIO-, METHYL ESTER

Base Information

Chemical Name:CARBANILIC ACID, p-BROMODITHIO-, METHYL ESTER
CAS No.:23121-37-1
Molecular Formula:C₈H₈BrNS₂
Molecular Weight:262.194
Hs Code.:
DSSTox Substance ID:DTXSID30177693
Mol file:23121-37-1.mol

Synonyms:Methyl p-bromodithiocarbanilate;23121-37-1;p-Bromodithiocarbanilic acid methyl ester;CARBANILIC ACID, p-BROMODITHIO-, METHYL ESTER;BRN 2803932;N-(4-bromophenyl)(methylsulfanyl)carbothioamide;4-12-00-01519 (Beilstein Handbook Reference);C8H8BrNS2;Maybridge3_000610;C8-H8-Br-N-S2;DTXSID30177693;PDHYVPIEZSMJRO-UHFFFAOYSA-N;HMS1432L16;CCG-43925;AKOS000269309;AKOS016035021;methyl (4-bromophenyl)carbamodithioate;IDI1_011997;LS-50884;SR-01000633800-1

Suppliers and Price of CARBANILIC ACID, p-BROMODITHIO-, METHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of CARBANILIC ACID, p-BROMODITHIO-, METHYL ESTER

Chemical Property:

Vapor Pressure:0.000238mmHg at 25°C
Boiling Point:324.9°Cat760mmHg
Flash Point:150.3°C
PSA：69.42000
Density:1.633g/cm³
LogP:3.58190
XLogP3:3.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:260.92815
Heavy Atom Count:12
Complexity:155

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CSC(=S)NC1=CC=C(C=C1)Br

Technology Process of CARBANILIC ACID, p-BROMODITHIO-, METHYL ESTER

There total 5 articles about CARBANILIC ACID, p-BROMODITHIO-, METHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 345923-51-5
methyl N-4-bromophenyl-N-formyldithiocarbamate

: 23121-37-1
methyl N-p-bromophenyldithiocarbamate

Guidance literature:: With aniline; In isopropyl alcohol; for 2h; Heating;

Reference yield:

: 2617-78-9
N-(4-bromophenyl)formamide

: 23121-37-1
methyl N-p-bromophenyldithiocarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: KOH / dimethylformamide / 25 - 28 °C

1.2: 41 percent / dimethylformamide / 10 - 40 °C

2.1: aniline / propan-2-ol / 2 h / Heating

With potassium hydroxide; aniline; In N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 106-40-1
4-bromo-aniline

: 23121-37-1
methyl N-p-bromophenyldithiocarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / dimethyl sulfoxide; water / 20 °C

2: dimethyl sulfoxide; water / 5 h / Cooling

With sodium hydroxide; In water; dimethyl sulfoxide;
DOI:10.1002/ardp.201500115