2-(trimethylsilyl)ethyl 3-O-allyl-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

Base Information

Chemical Name:2-(trimethylsilyl)ethyl 3-O-allyl-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside
CAS No.:192706-01-7
Molecular Formula:C₂₈H₃₈O₆Si
Molecular Weight:498.692
Hs Code.:

Synonyms:2-(trimethylsilyl)ethyl 3-O-allyl-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(trimethylsilyl)ethyl 3-O-allyl-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

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Technology Process of 2-(trimethylsilyl)ethyl 3-O-allyl-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

There total 2 articles about 2-(trimethylsilyl)ethyl 3-O-allyl-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 100-39-0
benzyl bromide

: 192706-00-6
2-(trimethylsilyl)ethyl 3-O-allyl-4,6-O-benzylidene-β-D-galactopyranoside

: 192706-01-7
2-(trimethylsilyl)ethyl 3-O-allyl-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 1h;
DOI:10.1080/07328309708007324

Reference yield:

: 189744-10-3
2-(trimethylsilyl)ethyl 4,6-O-benzylidene-β-D-galactopyranoside

: 192706-01-7
2-(trimethylsilyl)ethyl 3-O-allyl-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) dibutyltin oxide, 2.) tetrabutylammonium bromide / 1.) benzene, reflux, 24 h, 2.) reflux, 3 h

2: 85 percent / sodium hydride / dimethylformamide / 1 h / 0 °C

With tetrabutylammomium bromide; sodium hydride; di(n-butyl)tin oxide; In N,N-dimethyl-formamide;
DOI:10.1080/07328309708007324

Reference yield: 52.0%

: 192706-01-7
2-(trimethylsilyl)ethyl 3-O-allyl-2-O-benzyl-4,6-O-benzylidene-β-D-galactopyranoside

: 192706-02-8
2-(trimethylsilyl)ethyl 3-O-allyl-2,6-di-O-benzyl-β-D-galactopyranoside

Guidance literature:: With hydrogenchloride; molecular sieve; sodium cyanoborohydride; In tetrahydrofuran; diethyl ether; for 1h; Ambient temperature;
DOI:10.1080/07328309708007324