2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato cobalt(II)

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Chemical Name:2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato cobalt(II)
CAS No.:131214-89-6
Molecular Formula:C₄₄H₂₀Br₈CoN₄
Molecular Weight:1302.89
Hs Code.:

Synonyms:2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato cobalt(II)

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Chemical Property of 2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato cobalt(II)

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Technology Process of 2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato cobalt(II)

There total 3 articles about 2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato cobalt(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 71-48-7,917-69-1,5931-89-5,55881-15-7,68931-68-0,68931-69-1,93029-27-7
cobalt(II) acetate

: 2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenyl-21H,23H-porphyrin

: 131214-89-6
2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato cobalt(II)

Guidance literature:: In methanol; chloroform; for 1.5h; Reflux;
DOI:10.1134/S1070363216050182

Reference yield:

: 2,3,7,8,12,13,17,18-octobromo-5,10,15,20-tetraphenyl, 21H,23H-porphyrin

: 71-48-7,917-69-1,5931-89-5,55881-15-7,68931-68-0,68931-69-1,93029-27-7
cobalt(II) acetate

: 131214-89-6
2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato cobalt(II)

Guidance literature:: In N,N-dimethyl-formamide; treatment of C20H2N4(C6H5)4Br8 with excess of cobalt acetate in boiling DMF; chromy. on alumina with CHCl3 as an eluent;
DOI:10.1134/S0036023607020283

Reference yield:

: 917-23-7,20998-75-8
5,15,10,20-tetraphenylporphyrin

: 131214-89-6
2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato cobalt(II)

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide

2: chloroform; N,N-dimethyl-formamide; dichloromethane / 3 h / 20 °C

In dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1080/00958972.2021.1994963