N,N-(2,6-dimethyl-4-triisopropylsilanyloxyphenyl)-(3-iso-propyl-4-methoxymethoxyphenyl)amine

Base Information

Chemical Name:N,N-(2,6-dimethyl-4-triisopropylsilanyloxyphenyl)-(3-iso-propyl-4-methoxymethoxyphenyl)amine
CAS No.:852948-54-0
Molecular Formula:C₂₈H₄₅NO₃Si
Molecular Weight:471.756
Hs Code.:

Synonyms:N,N-(2,6-dimethyl-4-triisopropylsilanyloxyphenyl)-(3-iso-propyl-4-methoxymethoxyphenyl)amine

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Chemical Property of N,N-(2,6-dimethyl-4-triisopropylsilanyloxyphenyl)-(3-iso-propyl-4-methoxymethoxyphenyl)amine

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Technology Process of N,N-(2,6-dimethyl-4-triisopropylsilanyloxyphenyl)-(3-iso-propyl-4-methoxymethoxyphenyl)amine

There total 5 articles about N,N-(2,6-dimethyl-4-triisopropylsilanyloxyphenyl)-(3-iso-propyl-4-methoxymethoxyphenyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 852948-53-9
2,6-dimethyl-4-triisopropylsilanyloxyphenylamine

: 328236-42-6
4-bromo-2-isopropyl phenyl methoxymethyl ether

: 852948-54-0
N,N-(2,6-dimethyl-4-triisopropylsilanyloxyphenyl)-(3-iso-propyl-4-methoxymethoxyphenyl)amine

Guidance literature:: With potassium tert-butylate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In toluene; at 20 - 110 ℃; for 16.5h; sealed tube;

Reference yield:

: 88-69-7
2-(1-methylethyl)phenol

: 852948-54-0
N,N-(2,6-dimethyl-4-triisopropylsilanyloxyphenyl)-(3-iso-propyl-4-methoxymethoxyphenyl)amine

Guidance literature:: Multi-step reaction with 3 steps

1: bromine / dichloromethane / 0.75 h / 15 - 20 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 16.25 h / 15 - 20 °C / Heating / reflux

3: potassium tert-butylate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 16 h / 100 - 110 °C

With potassium tert-butylate; bromine; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; N-ethyl-N,N-diisopropylamine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In dichloromethane; toluene;

Reference yield:

: 13154-24-0
triisopropylsilyl chloride

: 852948-54-0
N,N-(2,6-dimethyl-4-triisopropylsilanyloxyphenyl)-(3-iso-propyl-4-methoxymethoxyphenyl)amine

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-imidazole / dichloromethane / 1 h / 20 °C

2: potassium tert-butylate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 16 h / 100 - 110 °C

With 1H-imidazole; potassium tert-butylate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In dichloromethane; toluene;