2,6-dimethyl-4-triisopropylsilanyloxyphenylamine

Base Information

Chemical Name:2,6-dimethyl-4-triisopropylsilanyloxyphenylamine
CAS No.:852948-53-9
Molecular Formula:C₁₇H₃₁NOSi
Molecular Weight:293.525
Hs Code.:

Synonyms:2,6-dimethyl-4-triisopropylsilanyloxyphenylamine

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Chemical Property of 2,6-dimethyl-4-triisopropylsilanyloxyphenylamine

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Technology Process of 2,6-dimethyl-4-triisopropylsilanyloxyphenylamine

There total 1 articles about 2,6-dimethyl-4-triisopropylsilanyloxyphenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 13154-24-0
triisopropylsilyl chloride

: 3096-70-6
3,5-dimethyl-4-aminophenol

: 852948-53-9
2,6-dimethyl-4-triisopropylsilanyloxyphenylamine

Guidance literature:: With 1H-imidazole; In dichloromethane; at 20 ℃; for 1h;

Reference yield: 58.0%

: 852948-53-9
2,6-dimethyl-4-triisopropylsilanyloxyphenylamine

: 328236-42-6
4-bromo-2-isopropyl phenyl methoxymethyl ether

: 852948-54-0
N,N-(2,6-dimethyl-4-triisopropylsilanyloxyphenyl)-(3-iso-propyl-4-methoxymethoxyphenyl)amine

Guidance literature:: With potassium tert-butylate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In toluene; at 20 - 110 ℃; for 16.5h; sealed tube;

Reference yield:

: 852948-53-9
2,6-dimethyl-4-triisopropylsilanyloxyphenylamine

: 852948-55-1
3,5-dimethyl-4-N-(3-iso-propyl-4'-methoxymethoxyphenylamino)phenol

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / toluene / 16 h / 100 - 110 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 16 h / 0 - 20 °C

With potassium tert-butylate; tetrabutyl ammonium fluoride; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In tetrahydrofuran; toluene;