trans,trans-benzoic acid 4-oxo-6-(trimethylsilanyl)-hexa-2,5-dienyl ester

Base Information

Chemical Name:trans,trans-benzoic acid 4-oxo-6-(trimethylsilanyl)-hexa-2,5-dienyl ester
CAS No.:862888-13-9
Molecular Formula:C₁₆H₂₀O₃Si
Molecular Weight:288.418
Hs Code.:

Synonyms:trans,trans-benzoic acid 4-oxo-6-(trimethylsilanyl)-hexa-2,5-dienyl ester

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Chemical Property of trans,trans-benzoic acid 4-oxo-6-(trimethylsilanyl)-hexa-2,5-dienyl ester

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Technology Process of trans,trans-benzoic acid 4-oxo-6-(trimethylsilanyl)-hexa-2,5-dienyl ester

There total 4 articles about trans,trans-benzoic acid 4-oxo-6-(trimethylsilanyl)-hexa-2,5-dienyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 862888-29-7
trans,trans-benzoic acid 4-hydroxy-6-(trimethylsilanyl)-hexa-2,5-dienyl ester

: 862888-13-9
trans,trans-benzoic acid 4-oxo-6-(trimethylsilanyl)-hexa-2,5-dienyl ester

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,4-dioxane; at 20 ℃; for 24h;
DOI:10.1081/SCC-200061633

Reference yield:

: 81121-63-3
4‐hydroxybut‐2‐en‐1‐yl benzoate

: 862888-13-9
trans,trans-benzoic acid 4-oxo-6-(trimethylsilanyl)-hexa-2,5-dienyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 51 percent / PCC; molecular sieves / CH₂Cl₂ / 2 h / 20 °C

2.1: Mg / tetrahydrofuran / 1 h / Heating

2.2: 74 percent / -43 - 25 °C

3.1: 99 percent / DDQ / dioxane / 24 h / 20 °C

With molecular sieve; magnesium; pyridinium chlorochromate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; 1,4-dioxane; dichloromethane;
DOI:10.1081/SCC-200061633

Reference yield:

: 118017-13-3
trans-benzoic acid 4-oxo-but-2-enyl ester

: 862888-13-9
trans,trans-benzoic acid 4-oxo-6-(trimethylsilanyl)-hexa-2,5-dienyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: Mg / tetrahydrofuran / 1 h / Heating

1.2: 74 percent / -43 - 25 °C

2.1: 99 percent / DDQ / dioxane / 24 h / 20 °C

With magnesium; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1081/SCC-200061633