C₂₃H₃₂O₇

Base Information

Chemical Name:C₂₃H₃₂O₇
CAS No.:1307264-22-7
Molecular Formula:C₂₃H₃₂O₇
Molecular Weight:420.503
Hs Code.:

C<sub>23</sub>H<sub>32</sub>O<sub>7</sub>

Synonyms:C₂₃H₃₂O₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₃₂O₇

Chemical Property:

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Technology Process of C₂₃H₃₂O₇

There total 1 articles about C₂₃H₃₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 925545-39-7
6-O-benzyl-1,2,3-trideoxy-4,5:7,8-di-O-isopropylidene-D-altro-oct-1-enitol

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 1307264-22-7
C₂₃H₃₂O₇

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; for 2h; Reflux;
DOI:10.1021/ol2009686

Reference yield: 73.0%

: 1307264-22-7
C₂₃H₃₂O₇

: 1307264-35-2
C₂₀H₂₈O₇

Guidance literature:: With water; acetic acid; at 20 ℃; for 7h; regioselective reaction;
DOI:10.1021/ol2009686

Reference yield:

: 1307264-22-7
C₂₃H₃₂O₇

: 50-36-2
Cocaine

Guidance literature:: Multi-step reaction with 10 steps

1.1: water; acetic acid / 7 h / 20 °C

2.1: sodium periodate; silica gel / dichloromethane / 0.5 h / 20 °C

3.1: triethylamine / toluene / 2 h / Reflux

3.2: 2 h / 20 °C

4.1: 2,4,6-trimethyl-pyridine / dichloromethane / 1 h / -78 °C

5.1: potassium carbonate / methanol / 0.17 h / 20 °C

6.1: hydrogen; acetic acid / methanol / 7 h / 20 - 60 °C

7.1: dmap; triethylamine / dichloromethane / 2 h / 0 °C

7.2: 1 h / 0 - 20 °C

8.1: hydrogen / methanol / 7 h / 50 °C

9.1: methanesulfonyl chloride; triethylamine / dichloromethane / 49 h / 0 - 70 °C / sealed tube

10.1: hydrogen / methanol / 14 h / 20 °C

With 2,4,6-trimethyl-pyridine; dmap; sodium periodate; water; hydrogen; silica gel; potassium carbonate; acetic acid; methanesulfonyl chloride; triethylamine; In methanol; dichloromethane; toluene;
DOI:10.1021/ol2009686