6-O-benzyl-1,2,3-trideoxy-4,5:7,8-di-O-isopropylidene-D-altro-oct-1-enitol

Base Information

Chemical Name:6-O-benzyl-1,2,3-trideoxy-4,5:7,8-di-O-isopropylidene-D-altro-oct-1-enitol
CAS No.:925545-39-7
Molecular Formula:C₂₁H₃₀O₅
Molecular Weight:362.466
Hs Code.:

Synonyms:6-O-benzyl-1,2,3-trideoxy-4,5:7,8-di-O-isopropylidene-D-altro-oct-1-enitol

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Chemical Property of 6-O-benzyl-1,2,3-trideoxy-4,5:7,8-di-O-isopropylidene-D-altro-oct-1-enitol

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Technology Process of 6-O-benzyl-1,2,3-trideoxy-4,5:7,8-di-O-isopropylidene-D-altro-oct-1-enitol

There total 3 articles about 6-O-benzyl-1,2,3-trideoxy-4,5:7,8-di-O-isopropylidene-D-altro-oct-1-enitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 925545-38-6
1,2,3-trideoxy-4,5:7,8-di-O-isopropylidene-D-altro-oct-1-enitol

: 100-39-0
benzyl bromide

: 925545-39-7
6-O-benzyl-1,2,3-trideoxy-4,5:7,8-di-O-isopropylidene-D-altro-oct-1-enitol

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1021/ol062621o

Reference yield:

: 912642-25-2
oct-7-ene-1,2,3,4,5-pentaol

: 925545-39-7
6-O-benzyl-1,2,3-trideoxy-4,5:7,8-di-O-isopropylidene-D-altro-oct-1-enitol

Guidance literature:: Multi-step reaction with 2 steps

1: 264 mg / anhydrous CuSO₄ / 24 h / 20 °C

2: 97 percent / sodium hydride; tetra-n-butylammonium iodide / tetrahydrofuran / 0 - 20 °C

With tetra-(n-butyl)ammonium iodide; sodium hydride; copper(II) sulfate; In tetrahydrofuran;
DOI:10.1021/ol062621o

Reference yield:

: 50-69-1
D-ribose

: 925545-39-7
6-O-benzyl-1,2,3-trideoxy-4,5:7,8-di-O-isopropylidene-D-altro-oct-1-enitol

Guidance literature:: Multi-step reaction with 3 steps

1: indium / ethanol / 12 h / 20 °C

2: 264 mg / anhydrous CuSO₄ / 24 h / 20 °C

3: 97 percent / sodium hydride; tetra-n-butylammonium iodide / tetrahydrofuran / 0 - 20 °C

With indium; tetra-(n-butyl)ammonium iodide; sodium hydride; copper(II) sulfate; In tetrahydrofuran; ethanol;
DOI:10.1021/ol062621o