trifluoro-methanesulfonic acid 1-cyclohexylidene-3-trimethylsilanyl-prop-2-ynyl ester

Base Information

Chemical Name:trifluoro-methanesulfonic acid 1-cyclohexylidene-3-trimethylsilanyl-prop-2-ynyl ester
CAS No.:244191-28-4
Molecular Formula:C₁₃H₁₉F₃O₃SSi
Molecular Weight:340.439
Hs Code.:

Synonyms:trifluoro-methanesulfonic acid 1-cyclohexylidene-3-trimethylsilanyl-prop-2-ynyl ester

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Chemical Property of trifluoro-methanesulfonic acid 1-cyclohexylidene-3-trimethylsilanyl-prop-2-ynyl ester

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Technology Process of trifluoro-methanesulfonic acid 1-cyclohexylidene-3-trimethylsilanyl-prop-2-ynyl ester

There total 1 articles about trifluoro-methanesulfonic acid 1-cyclohexylidene-3-trimethylsilanyl-prop-2-ynyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 53724-05-3
1-cyclohexyl-3-(trimethylsilyl)prop-2-yn-1-one

: 244191-28-4
trifluoro-methanesulfonic acid 1-cyclohexylidene-3-trimethylsilanyl-prop-2-ynyl ester

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; In dichloromethane; at 20 ℃;
DOI:10.1002/(SICI)1521-3773(19990712)38:13/14<1940::AID-ANIE1940>3.0.CO;2-8

Reference yield: 81.0%

: 89343-06-6
tris-iso-propylsilyl acetylene

: 244191-28-4
trifluoro-methanesulfonic acid 1-cyclohexylidene-3-trimethylsilanyl-prop-2-ynyl ester

: 483370-37-2
3-cyclohexylidene-1-triisopropylsilyl-5-trimethylsilylpenta-1,4-diyne

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; diethylamine; at 20 ℃; for 19h;
DOI:10.1002/1522-2675(200207)85:7<2169::AID-HLCA2169>3.0.CO;2-Z

Reference yield:

: 492461-51-5
3-ethynyl-4-methylpent-3-en-1-yne

: 244191-28-4
trifluoro-methanesulfonic acid 1-cyclohexylidene-3-trimethylsilanyl-prop-2-ynyl ester

: 244191-29-5
C₃₂H₄₄Si₂

Guidance literature:: With copper(l) iodide; diethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1002/(SICI)1521-3773(19990712)38:13/14<1940::AID-ANIE1940>3.0.CO;2-8