4-methoxy-N-[4-[(4-methoxyphenyl)sulfonylamino]-1-naphthyl]benzenesulfonamide

Base Information

• Chemical Name: 4-methoxy-N-[4-[(4-methoxyphenyl)sulfonylamino]-1-naphthyl]benzenesulfonamide
• CAS No.: 321694-20-6
• Molecular Formula: C₂₄H₂₂N₂O₆S₂
• Molecular Weight: 498.58

Synonyms:4-methoxy-N-[4-[(4-methoxyphenyl)sulfonylamino]-1-naphthyl]benzenesulfonamide

Chemical Property of 4-methoxy-N-[4-[(4-methoxyphenyl)sulfonylamino]-1-naphthyl]benzenesulfonamide

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Technology Process of 4-methoxy-N-[4-[(4-methoxyphenyl)sulfonylamino]-1-naphthyl]benzenesulfonamide

There total 4 articles about 4-methoxy-N-[4-[(4-methoxyphenyl)sulfonylamino]-1-naphthyl]benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1,4-diaminonaphthalene (2243-61-0) + 4-methoxy-phenyl-sulphonyl chloride (98-68-0) → 4-methoxy-N-[4-[(4-methoxyphenyl)sulfonylamino]-1-naphthyl]benzenesulfonamide (321694-20-6)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1016/j.bmcl.2016.10.083

Reference yield:

1-amino-4-nitronaphthalene (776-34-1) + 4-methoxy-phenyl-sulphonyl chloride (98-68-0) → 4-methoxy-N-[4-[(4-methoxyphenyl)sulfonylamino]-1-naphthyl]benzenesulfonamide (321694-20-6)

Guidance literature:

1-amino-4-nitronaphthalene; With palladium on activated charcoal; hydrogen; In tetrahydrofuran; at 20 ℃; for 4h;

4-methoxy-phenyl-sulphonyl chloride; With pyridine; In toluene; at 100 ℃; for 2h;

DOI:10.1016/j.redox.2020.101565

Reference yield:

1-amino-4-nitronaphthalene (776-34-1) → 4-methoxy-N-[4-[(4-methoxyphenyl)sulfonylamino]-1-naphthyl]benzenesulfonamide (321694-20-6)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogen; palladium on activated charcoal / tetrahydrofuran / 4 h / 20 °C

2: pyridine / toluene / 2 h / 100 °C / Inert atmosphere

With pyridine; palladium on activated charcoal; hydrogen; In tetrahydrofuran; toluene;

DOI:10.1021/jm5000529

upstream raw materials:

1,4-diaminonaphthalene

4-methoxy-phenyl-sulphonyl chloride

1-amino-4-nitronaphthalene

1-Nitronaphthalene

Downstream raw materials:

2,2′-(naphthalene-1,4-diylbis(((4-methoxyphenyl)sulfonyl)azanediyl))diacetic acid

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