(S)-ethyl 3-(3-bromo-5-(tert-butyl)phenyl)-3-(2-(3-guanidinobenzamido)acetamido)propanoate

Base Information

Chemical Name:(S)-ethyl 3-(3-bromo-5-(tert-butyl)phenyl)-3-(2-(3-guanidinobenzamido)acetamido)propanoate
CAS No.:1541198-84-8
Molecular Formula:C₂₅H₃₂BrN₅O₄
Molecular Weight:546.464
Hs Code.:

Synonyms:(S)-ethyl 3-(3-bromo-5-(tert-butyl)phenyl)-3-(2-(3-guanidinobenzamido)acetamido)propanoate

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Chemical Property of (S)-ethyl 3-(3-bromo-5-(tert-butyl)phenyl)-3-(2-(3-guanidinobenzamido)acetamido)propanoate

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Technology Process of (S)-ethyl 3-(3-bromo-5-(tert-butyl)phenyl)-3-(2-(3-guanidinobenzamido)acetamido)propanoate

There total 12 articles about (S)-ethyl 3-(3-bromo-5-(tert-butyl)phenyl)-3-(2-(3-guanidinobenzamido)acetamido)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1541197-63-0
(S)-3-(2-aminoacetylamino)-3-(3-bromo-5-tert-butylphenyl)propionic acid ethyl ester hydrochloride salt

: 82957-07-1
3-Guanidinobenzoic acid

: 1541198-84-8
(S)-ethyl 3-(3-bromo-5-(tert-butyl)phenyl)-3-(2-(3-guanidinobenzamido)acetamido)propanoate

Guidance literature:: (S)-3-(2-aminoacetylamino)-3-(3-bromo-5-tert-butylphenyl)propionic acid ethyl ester hydrochloride salt; 3-Guanidinobenzoic acid; With benzotriazol-1-ol; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 0.166667h; Inert atmosphere;

With diisopropyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;

Reference yield:

: 433704-66-6
3-(3-benzoylthioureido)benzoic acid

: 1541198-84-8
(S)-ethyl 3-(3-bromo-5-(tert-butyl)phenyl)-3-(2-(3-guanidinobenzamido)acetamido)propanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium methylate / methanol / 1 h / 20 °C

2.1: ethanol / 5 h / Reflux

3.1: ammonium hydroxide / 3 h / Reflux

4.1: benzotriazol-1-ol / N,N-dimethyl-formamide; dichloromethane / 0.17 h / 20 °C / Inert atmosphere

4.2: 20 °C / Inert atmosphere

With ammonium hydroxide; sodium methylate; benzotriazol-1-ol; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 37182-75-5
1-(3-carboxyphenyl)-2-thiourea

: 1541198-84-8
(S)-ethyl 3-(3-bromo-5-(tert-butyl)phenyl)-3-(2-(3-guanidinobenzamido)acetamido)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol / 5 h / Reflux

2.1: ammonium hydroxide / 3 h / Reflux

3.1: benzotriazol-1-ol / N,N-dimethyl-formamide; dichloromethane / 0.17 h / 20 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

With ammonium hydroxide; benzotriazol-1-ol; In ethanol; dichloromethane; N,N-dimethyl-formamide;