Technology Process of (3S,4R,5S,6R)-(-)-3,4,5-Tris-6-phthalimidocyclohexene
There total 6 articles about (3S,4R,5S,6R)-(-)-3,4,5-Tris-6-phthalimidocyclohexene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1H-imidazole;
In
dichloromethane;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 90 percent / Na2CO3, CaSO4 / acetone / 24 h / 30 °C
2: 92 percent / 80percent AcOH / 2 h / 65 °C
3: 98 percent / imidazole / CH2Cl2 / Ambient temperature
With
1H-imidazole; calcium sulfate; sodium carbonate; acetic acid;
In
dichloromethane; acetone;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 82 percent / diethyl ether; CH2Cl2; ethanol / 168 h / -30 °C
2: 94 percent / Al/Hg / tetrahydrofuran; H2O / 48 h / 0 °C
3: 90 percent / Na2CO3, CaSO4 / acetone / 24 h / 30 °C
4: 92 percent / 80percent AcOH / 2 h / 65 °C
5: 98 percent / imidazole / CH2Cl2 / Ambient temperature
With
1H-imidazole; calcium sulfate; aluminum amalgam; sodium carbonate; acetic acid;
In
tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; acetone;