N-(carboxymethylcarbonyl) α-(9-fluorenylmethyl) β-cyclohexyl L-aspartate

Base Information

Chemical Name:N-(carboxymethylcarbonyl) α-(9-fluorenylmethyl) β-cyclohexyl L-aspartate
CAS No.:330187-49-0
Molecular Formula:C₂₇H₂₉NO₇
Molecular Weight:479.53
Hs Code.:

Synonyms:N-(carboxymethylcarbonyl) α-(9-fluorenylmethyl) β-cyclohexyl L-aspartate

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Chemical Property of N-(carboxymethylcarbonyl) α-(9-fluorenylmethyl) β-cyclohexyl L-aspartate

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Technology Process of N-(carboxymethylcarbonyl) α-(9-fluorenylmethyl) β-cyclohexyl L-aspartate

There total 2 articles about N-(carboxymethylcarbonyl) α-(9-fluorenylmethyl) β-cyclohexyl L-aspartate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 446880-42-8
N-(tert-butyloxycarbonylmethylcarbonyl) α-(9-fluorenylmethyl) β-cyclohexyl L-aspartate

: 330187-49-0
N-(carboxymethylcarbonyl) α-(9-fluorenylmethyl) β-cyclohexyl L-aspartate

Guidance literature:: With hydrogenchloride; In diethyl ether; at 20 ℃;
DOI:10.1021/jo011041w

Reference yield:

: 1-α-(9-fluorenylmethyl)-β-cyclohexyl-aspartate hydrochloride

: 330187-49-0
N-(carboxymethylcarbonyl) α-(9-fluorenylmethyl) β-cyclohexyl L-aspartate

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / DCC; diisopropylethylamine / CH₂Cl₂ / 0.5 h / 20 °C

2: HCl / diethyl ether / 20 °C

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In diethyl ether; dichloromethane;
DOI:10.1021/jo011041w

Reference yield:

: 330187-49-0
N-(carboxymethylcarbonyl) α-(9-fluorenylmethyl) β-cyclohexyl L-aspartate

: 330187-58-1
3-phenyl-1(S)-[[2'-[N''-(9-fluorenylmethoxycarbonyl)-N''-(tert-butyloxycarbonylmethyl)]amino]ethylamino]propionamide

: 2-{2-[{2-[tert-butoxycarbonylmethyl-(9H-fluoren-9-ylmethoxycarbonyl)-amino]-ethyl}-(1-carbamoyl-2-phenyl-ethyl)-carbamoyl]-acetylamino}-succinic acid 4-cyclohexyl ester 1-(9H-fluoren-9-ylmethyl) ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 4h;
DOI:10.1021/jo011041w