10-[(2S,4S,5S,6R)-5-hydroxy-6-(hydroxymethyl)-2-phenyl-1,3-dioxan-4-yl]methyl-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione

Base Information

Chemical Name:10-[(2S,4S,5S,6R)-5-hydroxy-6-(hydroxymethyl)-2-phenyl-1,3-dioxan-4-yl]methyl-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione
CAS No.:278793-03-6
Molecular Formula:C₂₄H₂₄N₄O₆
Molecular Weight:464.478
Hs Code.:

Synonyms:10-[(2S,4S,5S,6R)-5-hydroxy-6-(hydroxymethyl)-2-phenyl-1,3-dioxan-4-yl]methyl-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione

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Chemical Property of 10-[(2S,4S,5S,6R)-5-hydroxy-6-(hydroxymethyl)-2-phenyl-1,3-dioxan-4-yl]methyl-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione

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Technology Process of 10-[(2S,4S,5S,6R)-5-hydroxy-6-(hydroxymethyl)-2-phenyl-1,3-dioxan-4-yl]methyl-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione

There total 1 articles about 10-[(2S,4S,5S,6R)-5-hydroxy-6-(hydroxymethyl)-2-phenyl-1,3-dioxan-4-yl]methyl-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1125-88-8
benzaldehyde dimethyl acetal

: 83-88-5,42880-33-1
riboflavin

: 278793-03-6
10-[(2S,4S,5S,6R)-5-hydroxy-6-(hydroxymethyl)-2-phenyl-1,3-dioxan-4-yl]methyl-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione

Guidance literature:: With camphor-10-sulfonic acid; In N,N-dimethyl-formamide;
DOI:10.1021/ol005739s

Reference yield: 95.0%

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 278793-03-6
10-[(2S,4S,5S,6R)-5-hydroxy-6-(hydroxymethyl)-2-phenyl-1,3-dioxan-4-yl]methyl-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione

: 603991-76-0
10-[((2S,4S,5S,6R)-6-[bis(4-methoxyphenyl)(phenyl)methoxy]methyl-5-hydroxy-2-phenyl-1,3-dioxan-4-yl)methyl]-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione

Guidance literature:: With pyridine; at 20 ℃; for 2h;
DOI:10.1016/j.bioorg.2020.104213

Reference yield: 85.0%

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 15715-58-9
triethylamine carbonate

: 278793-03-6
10-[(2S,4S,5S,6R)-5-hydroxy-6-(hydroxymethyl)-2-phenyl-1,3-dioxan-4-yl]methyl-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione

: C₁₇H₂₀N₄O₆C₂₈H₂₃O₄P*C₆H₁₅N

Guidance literature:: 4,4'-dimethoxytrityl chloride; 10-[(2S,4S,5S,6R)-5-hydroxy-6-(hydroxymethyl)-2-phenyl-1,3-dioxan-4-yl]methyl-7,8-dimethylbenzo[g]pteridine-2,4(3H,10H)-dione; With pyridine;

With 1H-tetrazole; N-ethyl-N,N-diisopropylamine; phosphorus trichloride;

triethylamine carbonate; pH=7.7; Further stages.;
DOI:10.1021/ol005739s