tricyclo[3.2.1.0~2,4~]octan-8-one

Base Information

Chemical Name:tricyclo[3.2.1.0~2,4~]octan-8-one
CAS No.:14224-86-3
Molecular Formula:C8H10 O
Molecular Weight:122.1644
Hs Code.:
Mol file:14224-86-3.mol

Synonyms:Tricyclo[3.2.1.02,4]octan-8-one,(1a,2a,4a,5a)-;Tricyclo[3.2.1.02,4]octan-8-one, endo- (8CI); endo-Tricyclo[3.2.1.02,4]octan-8-one

Suppliers and Price of tricyclo[3.2.1.0~2,4~]octan-8-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of tricyclo[3.2.1.0~2,4~]octan-8-one

Chemical Property:

Vapor Pressure:0.145mmHg at 25°C
Boiling Point:215.8°Cat760mmHg
Flash Point:77.2°C
Density:1.215g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of tricyclo[3.2.1.0~2,4~]octan-8-one

There total 13 articles about tricyclo[3.2.1.0~2,4~]octan-8-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14224-62-5,22479-17-0
1.5.6.7-Tetrachlor-8.8-dimethoxy-exo-tricyclo<3.2.1.0^2.4>-octen-(6)

: 14224-86-3
endo-Tricyclo<3.2.1.0^2,4>octane-8-one

Guidance literature:: Multi-step reaction with 2 steps

1: Li / tetrahydrofuran; 2-methyl-propan-2-ol

2: aq. HClO₄ / tetrahydrofuran

With perchloric acid; lithium; In tetrahydrofuran; tert-butyl alcohol;
DOI:10.1016/S0040-4020(01)82700-9

Reference yield:

: 2207-27-4
5,5-dimethoxy-1,2,3,4-tetrachlorocyclopentadiene

: 14224-86-3
endo-Tricyclo<3.2.1.0^2,4>octane-8-one

Guidance literature:: Multi-step reaction with 3 steps

1: petroleum ether

2: Li / tetrahydrofuran; 2-methyl-propan-2-ol

3: aq. HClO₄ / tetrahydrofuran

With perchloric acid; lithium; In tetrahydrofuran; Petroleum ether; tert-butyl alcohol;
DOI:10.1016/S0040-4020(01)82700-9

Reference yield:

: 8,8-Dimethoxy-endo-tricyclo<3.2.1.0^2,4>oct-6-en

: 14224-86-3
endo-Tricyclo<3.2.1.0^2,4>octane-8-one

Guidance literature:: Multi-step reaction with 2 steps

1: (catalytic hydrogenation)

2: H⁺

With hydrogen cation;
DOI:10.1021/ja00984a037