1,6-bis(6-bromo-3,4-dimethoxyphenyl)hextane

Base Information

Chemical Name:1,6-bis(6-bromo-3,4-dimethoxyphenyl)hextane
CAS No.:1115271-77-6
Molecular Formula:C₂₂H₂₈Br₂O₄
Molecular Weight:516.27
Hs Code.:

Synonyms:1,6-bis(6-bromo-3,4-dimethoxyphenyl)hextane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,6-bis(6-bromo-3,4-dimethoxyphenyl)hextane

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Technology Process of 1,6-bis(6-bromo-3,4-dimethoxyphenyl)hextane

There total 4 articles about 1,6-bis(6-bromo-3,4-dimethoxyphenyl)hextane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 51487-60-6
1,6-bis(3,4-dimethoxyphenyl)hexane

: 1115271-77-6
1,6-bis(6-bromo-3,4-dimethoxyphenyl)hextane

Guidance literature:: With bromine; In dichloromethane;
DOI:10.1055/s-0028-1083232

Reference yield:

: 50766-16-0
1,6-bis(3,4-dimethoxyphenyl)-1,6-hexanedione

: 1115271-77-6
1,6-bis(6-bromo-3,4-dimethoxyphenyl)hextane

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen; perchloric acid / ethyl acetate / 2 h / 22 °C / 2327.23 Torr / Inert atmosphere

2: bromine / dichloromethane / 1 h / 22 °C / Inert atmosphere

With perchloric acid; palladium 10% on activated carbon; hydrogen; bromine; In dichloromethane; ethyl acetate;
DOI:10.1002/anie.201609695

Reference yield:

: 91-16-7
1,2-dimethoxybenzene

: 1115271-77-6
1,6-bis(6-bromo-3,4-dimethoxyphenyl)hextane

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride / dichloromethane / 14 h / -10 - 0 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen; perchloric acid / ethyl acetate / 2 h / 22 °C / 2327.23 Torr / Inert atmosphere

3: bromine / dichloromethane / 1 h / 22 °C / Inert atmosphere

With aluminum (III) chloride; perchloric acid; palladium 10% on activated carbon; hydrogen; bromine; In dichloromethane; ethyl acetate;
DOI:10.1002/anie.201609695