7-<2-hydroxy-3-amino>propoxy>flavone

Base Information

Chemical Name:7-<2-hydroxy-3-amino>propoxy>flavone
CAS No.:117096-66-9
Molecular Formula:C₂₉H₂₉NO₆
Molecular Weight:487.552
Hs Code.:

7-<2-hydroxy-3-<N-propyl-N-<(benzyloxy)carbonyl>amino>propoxy>flavone

Synonyms:7-<2-hydroxy-3-amino>propoxy>flavone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-<2-hydroxy-3-amino>propoxy>flavone

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Technology Process of 7-<2-hydroxy-3-amino>propoxy>flavone

There total 9 articles about 7-<2-hydroxy-3-amino>propoxy>flavone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 79619-31-1
7-(3-n-propylamino-2-hydroxypropoxy)-flavone

: 117096-66-9
7-<2-hydroxy-3-amino>propoxy>flavone

Guidance literature:: With triethylamine; In dichloromethane; for 4h; Heating;
DOI:10.1021/jm00121a034

Reference yield:

: 89-84-9
2',4'-dihydroxy-4-acetophenone

: 117096-66-9
7-<2-hydroxy-3-amino>propoxy>flavone

Guidance literature:: Multi-step reaction with 6 steps

1: 63 percent / K₂CO₃ / acetone / Heating

2: 85 percent / NaOAc, glacial acetic acid / 16 h / Heating

3: 72 percent / NaOH / H₂O; propan-2-ol / 2 h / 70 °C

5: 86 percent / H₂, HOAc / 10percentPd/C / methanol

6: 52 percent / NEt₃ / CH₂Cl₂ / 4 h / Heating

With sodium hydroxide; hydrogen; sodium acetate; potassium carbonate; acetic acid; triethylamine; 10% palladium on active carbon; In methanol; dichloromethane; water; isopropyl alcohol; acetone;
DOI:10.1021/jm00121a034

Reference yield:

: 93-97-0
benzoic acid anhydride

: 117096-66-9
7-<2-hydroxy-3-amino>propoxy>flavone

Guidance literature:: Multi-step reaction with 5 steps

1: 1) Na-benzoate, 2) KOH / 1) 180-190 deg C, 6 h, 2) C₂H₅OH, H₂O, reflux, 30 min

2: 72 percent / NaOH / H₂O; propan-2-ol / 2 h / 70 °C

4: 86 percent / H₂, HOAc / 10percentPd/C / methanol

5: 52 percent / NEt₃ / CH₂Cl₂ / 4 h / Heating

With sodium benzoate; potassium hydroxide; sodium hydroxide; hydrogen; acetic acid; triethylamine; 10% palladium on active carbon; In methanol; dichloromethane; water; isopropyl alcohol;
DOI:10.1021/jm00121a034