2a,2b,6b,6c-Tetrahydro-1-oxa-2-thiabenzocyclopropapentalene 2-Oxide

Base Information

• Chemical Name: 2a,2b,6b,6c-Tetrahydro-1-oxa-2-thiabenzo
• Molecular Formula: C₁₀H₈O₂S
• Molecular Weight: 192.238

Synonyms:2a,2b,6b,6c-Tetrahydro-1-oxa-2-thiabenzocyclopropapentalene 2-Oxide

Chemical Property of 2a,2b,6b,6c-Tetrahydro-1-oxa-2-thiabenzo

Chemical Property:

Purity/Quality:

80%，90%，95%，98%，99% ^*data from raw suppliers

Safty Information:

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Useful:

There total 1 articles about 2a,2b,6b,6c-Tetrahydro-1-oxa-2-thiabenzocyclopropapentalene 2-Oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1a,6,6a-Tetrahydro-1,6-epithiocyclopropindene 7,7-Dioxide (122608-25-7) → naphthalene (91-20-3,71998-51-1,72931-45-4) + 2a,2b,6b,6c-Tetrahydro-1-oxa-2-thiabenzocyclopropapentalene 2-Oxide (122608-26-8) + 1H-indene-1-carboxaldehyde (60585-47-9) + 1H-indene-3-carboxaldehyde (64391-31-7)

Guidance literature:

at 376.9 ℃; under 5E-06 Torr; Yield given. Yields of byproduct given;

DOI:10.1016/S0040-4039(00)99128-7

Reference yield:

2a,2b,6b,6c-Tetrahydro-1-oxa-2-thiabenzocyclopropapentalene 2-Oxide (122608-26-8) → naphthalene (91-20-3,71998-51-1,72931-45-4) + 1H-indene-1-carboxaldehyde (60585-47-9) + 1H-indene-3-carboxaldehyde (64391-31-7) + 1-indene (95-13-6)

Guidance literature:

at 476.9 ℃; under 5E-06 Torr; Mechanism; Product distribution; effect of different reaction temperature was investigated;

DOI:10.1016/S0040-4039(00)99128-7

Reference yield:

2a,2b,6b,6c-Tetrahydro-1-oxa-2-thiabenzocyclopropapentalene 2-Oxide (122608-26-8) → naphthalene (91-20-3,71998-51-1,72931-45-4) + 1,2,3-metheno-1H-indene-2,3-dihydro (34305-47-0) + 1,1a,6,6a-Tetrahydro-1,6-epithiocyclopropindene 7,7-Dioxide (122608-25-7)

Guidance literature:

With pyridine; In ⁽²⁾H₈-toluene; at -75 ℃; Mechanism; Irradiation;

DOI:10.1002/hlca.19900730617

upstream raw materials:

1,1a,6,6a-Tetrahydro-1,6-epithiocyclopropindene 7,7-Dioxide

Downstream raw materials:

naphthalene

1,2,3-metheno-1H-indene-2,3-dihydro

1,1a,6,6a-Tetrahydro-1,6-epithiocyclopropindene 7,7-Dioxide

1H-indene-1-carboxaldehyde

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