Benzyl-hydroxymethyl-dithiocarbamic acid hydroxymethyl ester

Base Information

• Chemical Name: Benzyl-hydroxymethyl-dithiocarbamic acid hydroxymethyl ester
• CAS No.: 1027986-95-3
• Molecular Formula: C₁₀H₁₃NO₂S₂
• Molecular Weight: 243.351
• Mol file: 1027986-95-3.mol

Synonyms:Benzyl-hydroxymethyl-dithiocarbamic acid hydroxymethyl ester

Chemical Property of Benzyl-hydroxymethyl-dithiocarbamic acid hydroxymethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzyl-hydroxymethyl-dithiocarbamic acid hydroxymethyl ester

There total 4 articles about Benzyl-hydroxymethyl-dithiocarbamic acid hydroxymethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + potassium benzylcarbamodithioate (1950-25-0) → Benzyl-hydroxymethyl-dithiocarbamic acid hydroxymethyl ester (1027986-95-3)

Guidance literature:

In ethanol; water; for 1h; Ambient temperature;

DOI:10.1002/ardp.19973301103

Reference yield:

benzylamine (100-46-9) → Benzyl-hydroxymethyl-dithiocarbamic acid hydroxymethyl ester (1027986-95-3)

Guidance literature:

Multi-step reaction with 2 steps

1: KOH / ethanol / 3 h / 20 °C

2: ethanol / 1 h

With potassium hydroxide; In ethanol;

DOI:10.1002/1521-4184(200212)335:9<438::AID-ARDP438>3.0.CO;2-E

Reference yield:

benzylamine (100-46-9) → Benzyl-hydroxymethyl-dithiocarbamic acid hydroxymethyl ester (1027986-95-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 20percent KOH / ethanol / 3 h / Ambient temperature

2: ethanol; H₂O / 1 h / Ambient temperature

With potassium hydroxide; In ethanol; water;

DOI:10.1002/ardp.19973301103

upstream raw materials:

formaldehyd

potassium benzylcarbamodithioate

benzylamine

Downstream raw materials:

3-benzyl-5-(carboxymethyl)tetrahydro-(2H)-1,3,5-thiadiazine-2-thione

[2-(5-Benzyl-6-thioxo-[1,3,5]thiadiazinan-3-yl)-acetylamino]-acetic acid

3-benzyl-5-(2-hydroxyethyl)-3,4,5,6-tetrahydro-2H-1,3,5-thiadiazine-2-thione