N-(t-butoxycarbonyl)-3-[3-piperidyl-(N-guanidino (bis-benzyloxycarbonyl))]-L-alaninol

Base Information

Chemical Name:N-(t-butoxycarbonyl)-3-[3-piperidyl-(N-guanidino (bis-benzyloxycarbonyl))]-L-alaninol
CAS No.:195204-15-0
Molecular Formula:C₃₀H₄₀N₄O₇
Molecular Weight:568.67
Hs Code.:

Synonyms:N-(t-butoxycarbonyl)-3-[3-piperidyl-(N-guanidino (bis-benzyloxycarbonyl))]-L-alaninol

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Chemical Property of N-(t-butoxycarbonyl)-3-[3-piperidyl-(N-guanidino (bis-benzyloxycarbonyl))]-L-alaninol

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Technology Process of N-(t-butoxycarbonyl)-3-[3-piperidyl-(N-guanidino (bis-benzyloxycarbonyl))]-L-alaninol

There total 4 articles about N-(t-butoxycarbonyl)-3-[3-piperidyl-(N-guanidino (bis-benzyloxycarbonyl))]-L-alaninol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 25508-20-7
1,3-bis(benzyloxycarbonyl)-2-methylisothiourea

: ((S)-1-Hydroxymethyl-2-piperidin-3-yl-ethyl)-carbamic acid tert-butyl ester; compound with acetic acid

: 195204-15-0
N-(t-butoxycarbonyl)-3-[3-piperidyl-(N-guanidino (bis-benzyloxycarbonyl))]-L-alaninol

Guidance literature:: With 4-methyl-morpholine; In tetrahydrofuran;
DOI:10.1021/jm960607j

Reference yield:

: 195204-14-9
N-(t-butoxycarbonyl)-3-[3-piperidyl-(N-guanidino (bis-benzyloxycarbonyl))]-L-alanine methyl ester

: 195204-15-0
N-(t-butoxycarbonyl)-3-[3-piperidyl-(N-guanidino (bis-benzyloxycarbonyl))]-L-alaninol

Guidance literature:: With sodium tetrahydroborate; calcium chloride; In tetrahydrofuran; ethanol; at 20 ℃; for 12h;

Reference yield:

: 167298-45-5
(S)-[1-(hydroxymethyl)-2-(3-pyridinyl)ethyl]carbamic acid 1,1-dimethylethyl ester

: 195204-15-0
N-(t-butoxycarbonyl)-3-[3-piperidyl-(N-guanidino (bis-benzyloxycarbonyl))]-L-alaninol

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / 10percent PtO₂ / methanol / 2068.6 Torr

2: 82 percent / NMM / tetrahydrofuran

With 4-methyl-morpholine; hydrogen; platinum(IV) oxide; In tetrahydrofuran; methanol;
DOI:10.1021/jm960607j