Technology Process of C31H44BrN5O2Si
There total 12 articles about C31H44BrN5O2Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C20H24BrNO2;
With
N-ethyl-N,N-diisopropylamine; HATU;
In
dichloromethane;
at 0 ℃;
for 0.5h;
C11H22N4OSi;
In
dichloromethane;
at 10 ℃;
for 24h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C
1.2: 20 °C
2.1: hydrogen / palladium 10% on activated carbon / ethanol / 6 h / 20 °C / 760.05 Torr
3.1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 0.5 h / 0 °C
3.2: 24 h / 10 °C / Reflux
With
hydrogen; sodium hydride; N-ethyl-N,N-diisopropylamine; HATU;
palladium 10% on activated carbon;
In
tetrahydrofuran; ethanol; dichloromethane; mineral oil;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: triethylamine / dichloromethane / 3 h / Inert atmosphere; Cooling with ice bath
2.1: sodium hydride / tetrahydrofuran / 20 °C / Inert atmosphere
2.2: pH 3 / Ice water
3.1: hydrazine dihydrochloride / ethanol / 2.5 h / 60 °C
4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C
4.2: 20 °C
5.1: hydrogen / palladium 10% on activated carbon / ethanol / 6 h / 20 °C / 760.05 Torr
6.1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 0.5 h / 0 °C
6.2: 24 h / 10 °C / Reflux
With
hydrazine dihydrochloride; hydrogen; sodium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; HATU;
palladium 10% on activated carbon;
In
tetrahydrofuran; ethanol; dichloromethane; mineral oil;