((2R,3R,4S,5R)-3,4,5,6-tetraki s(benzyloxy)tetrahydro-2H-pyran-2-yl)methanol

Base Information

Chemical Name:((2R,3R,4S,5R)-3,4,5,6-tetraki s(benzyloxy)tetrahydro-2H-pyran-2-yl)methanol
CAS No.:61277-58-5
Molecular Formula:C₃₄H₃₆O₆
Molecular Weight:540.656
Hs Code.:

Synonyms:((2R,3R,4S,5R)-3,4,5,6-tetraki s(benzyloxy)tetrahydro-2H-pyran-2-yl)methanol

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Chemical Property of ((2R,3R,4S,5R)-3,4,5,6-tetraki s(benzyloxy)tetrahydro-2H-pyran-2-yl)methanol

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Technology Process of ((2R,3R,4S,5R)-3,4,5,6-tetraki s(benzyloxy)tetrahydro-2H-pyran-2-yl)methanol

There total 10 articles about ((2R,3R,4S,5R)-3,4,5,6-tetraki s(benzyloxy)tetrahydro-2H-pyran-2-yl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1423019-40-2
benzyl 2,3,4-tri-O-benzyl-6-tert-butyldimethylsilyl-D-glucopyranoside

: 61277-58-5
((2R,3R,4S,5R)-3,4,5,6-tetraki s(benzyloxy)tetrahydro-2H-pyran-2-yl)methanol

Guidance literature:: With sulfuric acid; sodium carbonate; In methanol; at 20 ℃;
DOI:10.1016/j.carres.2012.11.021

Reference yield: 59.0%

: C₃₇H₄₀O₆

: C₃₇H₄₂O₇

: 61277-58-5
((2R,3R,4S,5R)-3,4,5,6-tetraki s(benzyloxy)tetrahydro-2H-pyran-2-yl)methanol

Guidance literature:: C₃₇H₄₀O₆; With sodium tetrahydroborate; In tetrahydrofuran; for 0.166667h; Inert atmosphere;

With boron trifluoride diethyl etherate; In tetrahydrofuran; for 6h; Inert atmosphere;

With dihydrogen peroxide; sodium hydroxide; at 0 ℃; for 0.5h;
DOI:10.1002/anie.201510551

Reference yield:

: 2280-44-6
D-Glucose

: 61277-58-5
((2R,3R,4S,5R)-3,4,5,6-tetraki s(benzyloxy)tetrahydro-2H-pyran-2-yl)methanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 24 h / 20 °C

1.2: 1.5 h

2.1: acetic anhydride; acetic acid; zinc(II) chloride / 1.5 h

2.2: 5 h

With acetic anhydride; sodium hydride; acetic acid; zinc(II) chloride; In N,N-dimethyl-formamide; mineral oil;
DOI:10.2174/157017812801322390