methyl 3,4-O-isopropylidene-6-O-tert-butyldiphenylsilyl-α-D-galactopyranoside

Base Information

Chemical Name:methyl 3,4-O-isopropylidene-6-O-tert-butyldiphenylsilyl-α-D-galactopyranoside
CAS No.:114217-36-6
Molecular Formula:C₂₆H₃₆O₆Si
Molecular Weight:472.654
Hs Code.:

Synonyms:methyl 3,4-O-isopropylidene-6-O-tert-butyldiphenylsilyl-α-D-galactopyranoside

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Chemical Property of methyl 3,4-O-isopropylidene-6-O-tert-butyldiphenylsilyl-α-D-galactopyranoside

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Technology Process of methyl 3,4-O-isopropylidene-6-O-tert-butyldiphenylsilyl-α-D-galactopyranoside

There total 2 articles about methyl 3,4-O-isopropylidene-6-O-tert-butyldiphenylsilyl-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 40269-01-0
methyl 3,4-O-isopropylidene-α-D-galactopyranoside

: 114217-36-6
methyl 3,4-O-isopropylidene-6-O-tert-butyldiphenylsilyl-α-D-galactopyranoside

Guidance literature:: With 4-methylpyridine-1-oxide; In dichloromethane; at 20 ℃; regioselective reaction; Molecular sieve;
DOI:10.1016/j.tetlet.2015.12.114

Reference yield: 90.0%

: 114217-37-7
Trifluoro-methanesulfonic acid (3aS,4R,6S,7R,7aS)-4-(tert-butyl-diphenyl-silanyloxymethyl)-6-methoxy-2,2-dimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yl ester

: 77-76-9
2,2-dimethoxy-propane

: 114217-36-6
methyl 3,4-O-isopropylidene-6-O-tert-butyldiphenylsilyl-α-D-galactopyranoside

Guidance literature:: With camphor-10-sulfonic acid; In acetone;
DOI:10.1016/S0040-4039(00)96272-5

Reference yield: 90.0%

: 2-(((2R,3S,4R,5R)-3,4-bis(benzyloxy)-5-((benzyloxy)methyl)tetrahydrofuran-2-yl)oxy)-5,5-dimethyl-1,3,2-dioxaphosphinane 2-oxide

: 114217-36-6
methyl 3,4-O-isopropylidene-6-O-tert-butyldiphenylsilyl-α-D-galactopyranoside

: (((3aS,4R,6S,7R,7aS)-7-(((2S,3S,4R,5R)-3,4-bis(benzyloxy)-5-((benzyloxy)methyl)tetrahydrofuran-2-yl)oxy)-6-methoxy-2,2-dimethyltetrahydro-4H-[1,3]dioxolo[4,5-c]pyran-4-yl)methoxy)(tert-butyl)diphenylsilane

Guidance literature:: With C₅₀H₅₅F₉N₆O₄S₂; at 40 ℃; for 18h; stereoselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1021/jacs.0c00335