C₅₈H₁₀₈BrIO₁₀Si₅

Base Information

Chemical Name:C₅₈H₁₀₈BrIO₁₀Si₅
CAS No.:749900-23-0
Molecular Formula:C₅₈H₁₀₈BrIO₁₀Si₅
Molecular Weight:1312.73
Hs Code.:

C<sub>58</sub>H<sub>108</sub>BrIO<sub>10</sub>Si<sub>5</sub>

Synonyms:C₅₈H₁₀₈BrIO₁₀Si₅

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Chemical Property of C₅₈H₁₀₈BrIO₁₀Si₅

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Technology Process of C₅₈H₁₀₈BrIO₁₀Si₅

There total 7 articles about C₅₈H₁₀₈BrIO₁₀Si₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 493033-92-4
6-bromo-3,4-bis-O-(tert-butyldimethylsilyl)-2,6-dideoxy-2-iodo-β-D-glucopyranosyl fluoride

: 749900-21-8
Benzoic acid (1R,2R,3R,4S,7R,8S,9R)-3-(tert-butyl-dimethyl-silanyloxy)-9-(diethyl-isopropyl-silanyloxy)-7-hydroxy-1-((S)-1-methoxy-3-trimethylsilanyl-prop-2-ynyl)-2,4,8-trimethyl-5-oxo-decyl ester

: 749900-23-0
C₅₈H₁₀₈BrIO₁₀Si₅

Guidance literature:: With silver perchlorate; tin(ll) chloride; In diethyl ether; at -10 ℃;
DOI:10.1021/ja048493l

Reference yield:

: 98-88-4
benzoyl chloride

: 749900-23-0
C₅₈H₁₀₈BrIO₁₀Si₅

Guidance literature:: Multi-step reaction with 5 steps

1.1: Et₃N; DMAP / CH₂Cl₂ / 3 h

2.1: 137 mg / aq. AcOH / tetrahydrofuran / 16 h

3.1: 105 mg / pyridine; Dess-Martin periodinane; H₂O / CH₂Cl₂ / 0.83 h

4.1: LHMDS; Et₃N; TMSCl / tetrahydrofuran / -78 °C

4.2: 59 percent / BF*OEt₂ / CH₂Cl₂

5.1: 42 percent / SnCl₂; AgClO₄ / diethyl ether / -10 °C

With pyridine; dmap; chloro-trimethyl-silane; water; silver perchlorate; Dess-Martin periodane; acetic acid; triethylamine; tin(ll) chloride; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; dichloromethane; 3.1: Dess-Martin oxidation;
DOI:10.1021/ja048493l

Reference yield:

: 6-bromo-3,4-bis-O-(tert-butyldimethylsilyl)-2,6-dideoxy-2-iodo-β-D-glucopyranosyl acetate

: 749900-23-0
C₅₈H₁₀₈BrIO₁₀Si₅

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrazine / methanol; diethyl ether; H₂O / 1.5 h / 0 °C

1.2: 78 percent / diethylaminosulfur trifluoride / CH₂Cl₂ / 0.5 h / 0 °C

2.1: 42 percent / SnCl₂; AgClO₄ / diethyl ether / -10 °C

With silver perchlorate; tin(ll) chloride; hydrazine; In methanol; diethyl ether; water;
DOI:10.1021/ja048493l