5-[(6-benzyloxy-5-nitro-pyridine-2-carbonyl)-amino]-6-isopropoxy-pyridine-2-carboxylic acid methyl ester

Base Information

Chemical Name:5-[(6-benzyloxy-5-nitro-pyridine-2-carbonyl)-amino]-6-isopropoxy-pyridine-2-carboxylic acid methyl ester
CAS No.:475272-83-4
Molecular Formula:C₂₃H₂₂N₄O₇
Molecular Weight:466.45
Hs Code.:

Synonyms:5-[(6-benzyloxy-5-nitro-pyridine-2-carbonyl)-amino]-6-isopropoxy-pyridine-2-carboxylic acid methyl ester

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Chemical Property of 5-[(6-benzyloxy-5-nitro-pyridine-2-carbonyl)-amino]-6-isopropoxy-pyridine-2-carboxylic acid methyl ester

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Technology Process of 5-[(6-benzyloxy-5-nitro-pyridine-2-carbonyl)-amino]-6-isopropoxy-pyridine-2-carboxylic acid methyl ester

There total 9 articles about 5-[(6-benzyloxy-5-nitro-pyridine-2-carbonyl)-amino]-6-isopropoxy-pyridine-2-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16013-85-7,136901-10-5
2,6-dicholoro-3-nitropyridine

: 475272-83-4
5-[(6-benzyloxy-5-nitro-pyridine-2-carbonyl)-amino]-6-isopropoxy-pyridine-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1.1: NH₃ / ethanol

1.2: NaNO₂; H₂SO₄

1.3: H₂O

2.1: Ag₂CO₃

3.1: [Pd(PPh₃)4]

4.1: O₃ / acetic acid

4.2: AgNO₃; KOH

5.1: (COCl)2 / dimethylformamide

6.1: DIEA

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; oxalyl dichloride; ammonia; ozone; N-ethyl-N,N-diisopropylamine; silver carbonate; In ethanol; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/anie.200390154

Reference yield:

: 92138-35-7
6-chloro-3-nitro-1H-pyridin-2-one

: 475272-83-4
5-[(6-benzyloxy-5-nitro-pyridine-2-carbonyl)-amino]-6-isopropoxy-pyridine-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: Ag₂CO₃

2.1: [Pd(PPh₃)4]

3.1: O₃ / acetic acid

3.2: AgNO₃; KOH

4.1: (COCl)2 / dimethylformamide

5.1: DIEA

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; oxalyl dichloride; ozone; N-ethyl-N,N-diisopropylamine; silver carbonate; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/anie.200390154

Reference yield:

: 186413-80-9
2-isopropoxy-3-nitro-6-vinylpyridine

: 475272-83-4
5-[(6-benzyloxy-5-nitro-pyridine-2-carbonyl)-amino]-6-isopropoxy-pyridine-2-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: O₃ / acetic acid

1.2: AgNO₃; KOH

2.1: PTSA

3.1: H₂ / Pd/C

4.1: DIEA

With hydrogen; toluene-4-sulfonic acid; ozone; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In acetic acid;
DOI:10.1002/anie.200390154