Technology Process of C23H21BrN4O3
There total 7 articles about C23H21BrN4O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine; sodium iodide;
In
N,N-dimethyl-formamide;
at 70 ℃;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: sodium carbonate / acetone / 16 h / 75 °C
1.2: 0.25 h / 65 °C
2.1: potassium carbonate / toluene / 16 h / Reflux
3.1: sodium hydride / N,N-dimethyl-formamide / 0.75 h / 20 °C
3.2: 2 h / 20 - 90 °C
4.1: ammonium acetate / 2 h / 140 °C
4.2: pH 8 / Heating
5.1: triethylamine / dichloromethane / 1 h / 20 °C
6.1: triethylamine; sodium iodide / N,N-dimethyl-formamide / 70 °C
With
ammonium acetate; sodium hydride; sodium carbonate; potassium carbonate; triethylamine; sodium iodide;
In
dichloromethane; N,N-dimethyl-formamide; acetone; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate / toluene / 16 h / Reflux
2.1: sodium hydride / N,N-dimethyl-formamide / 0.75 h / 20 °C
2.2: 2 h / 20 - 90 °C
3.1: ammonium acetate / 2 h / 140 °C
3.2: pH 8 / Heating
4.1: triethylamine / dichloromethane / 1 h / 20 °C
5.1: triethylamine; sodium iodide / N,N-dimethyl-formamide / 70 °C
With
ammonium acetate; sodium hydride; potassium carbonate; triethylamine; sodium iodide;
In
dichloromethane; N,N-dimethyl-formamide; toluene;