Fe[η5-C5H4C(NHC6H11)(NC6H11)]2

Base Information

Chemical Name:Fe[η5-C5H4C(NHC6H11)(NC6H11)]2
CAS No.:364342-74-5
Molecular Formula:C₃₆H₅₄FeN₄
Molecular Weight:598.699
Hs Code.:

Synonyms:Fe[η5-C5H4C(NHC6H11)(NC6H11)]2

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Chemical Property of Fe[η5-C5H4C(NHC6H11)(NC6H11)]2

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Technology Process of Fe[η5-C5H4C(NHC6H11)(NC6H11)]2

There total 2 articles about Fe[η5-C5H4C(NHC6H11)(NC6H11)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 102-54-5,55404-68-7
ferrocene

: 538-75-0
dicyclohexyl-carbodiimide

: 364342-74-5
Fe[η5-C5H4C(NHC6H11)(NC6H11)]2

Guidance literature:: With TMEDA; n-BuLi; In hexane; suspn. of ferrocene was treated with TMEDA followed by addition of BuLi,mixt. was stirred at 25°C overnight, then cooled to 0°C a nd treated with CyNCNCy in hexane, mixt. was stirred for 20 h at room temp.; soln. was decanted, ppt. was treated with Et2O and then with water, mixt. was stirred for 30 min, water was added and then Et2O, solvent was evapd., solid was recrystd. from hot hexanes; elem. anal.;
DOI:10.1016/S0020-1693(01)00454-6

Reference yield: 50.0%

: 102-54-5,55404-68-7
ferrocene

: 538-75-0
dicyclohexyl-carbodiimide

: 364342-74-5
Fe[η5-C5H4C(NHC6H11)(NC6H11)]2

: 185699-79-0
(C₅H₅)Fe(C₅H₄C(NC₆H₁₁)(NHC₆H₁₁))

Guidance literature:: With tert-butyl lithium; In tetrahydrofuran; a pentane soln. of t-butyllithium was added dropwise over 2 h at 0°C to a suspn. of ferrocene in THF-hexane, stirred overnight, a THF soln. of diimide was added dropwise over 30 min, stirred overnight; H2O was added dropwise, the orange soln. was decanted, evapd., sublimed at 65°C/1E-2 mmHg, crystd. from boiling hexane; elem. anal.;
DOI:10.1016/S0022-328X(01)00973-1