2-(ethoxycarbonyl)-3-methyl-4-(1-methyl-1H-imidazol-3-ium-3-yl)-5-(4-nitrophenyl)pyrrol-1-ide

Base Information

Chemical Name:2-(ethoxycarbonyl)-3-methyl-4-(1-methyl-1H-imidazol-3-ium-3-yl)-5-(4-nitrophenyl)pyrrol-1-ide
CAS No.:1619941-37-5
Molecular Formula:C₁₈H₁₈N₄O₄
Molecular Weight:354.365
Hs Code.:

Synonyms:2-(ethoxycarbonyl)-3-methyl-4-(1-methyl-1H-imidazol-3-ium-3-yl)-5-(4-nitrophenyl)pyrrol-1-ide

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Chemical Property of 2-(ethoxycarbonyl)-3-methyl-4-(1-methyl-1H-imidazol-3-ium-3-yl)-5-(4-nitrophenyl)pyrrol-1-ide

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Technology Process of 2-(ethoxycarbonyl)-3-methyl-4-(1-methyl-1H-imidazol-3-ium-3-yl)-5-(4-nitrophenyl)pyrrol-1-ide

There total 3 articles about 2-(ethoxycarbonyl)-3-methyl-4-(1-methyl-1H-imidazol-3-ium-3-yl)-5-(4-nitrophenyl)pyrrol-1-ide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1619941-08-0
3-(5-ethoxycarbonyl-4-methyl-2-(4-nitrophenyl)-1H-pyrrol-3-yl)-1-methyl-1H-imidazol-3-ium bromide

: 1619941-37-5
2-(ethoxycarbonyl)-3-methyl-4-(1-methyl-1H-imidazol-3-ium-3-yl)-5-(4-nitrophenyl)pyrrol-1-ide

Guidance literature:: With potassium hydroxide; In water; for 12h; Sonication;
DOI:10.1039/c4ob00865k

Reference yield:

: 99-81-0
4-Nitrophenacyl bromide

: 1619941-37-5
2-(ethoxycarbonyl)-3-methyl-4-(1-methyl-1H-imidazol-3-ium-3-yl)-5-(4-nitrophenyl)pyrrol-1-ide

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether / 12 h / 20 °C

2: triethylamine / dichloromethane / 19 h / Reflux

3: potassium hydroxide / water / 12 h / Sonication

With triethylamine; potassium hydroxide; In diethyl ether; dichloromethane; water;
DOI:10.1039/c4ob00865k

Reference yield:

: 59349-30-3
1-methyl-3-(2-(4-nitrophenyl)-2-oxoethyl)-1H-imidazol-3-ium bromide

: 14369-88-1
(±)-ethyl 3-methyl-2H-azirine-2-carboxylate

: 1619941-37-5
2-(ethoxycarbonyl)-3-methyl-4-(1-methyl-1H-imidazol-3-ium-3-yl)-5-(4-nitrophenyl)pyrrol-1-ide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 19 h / Reflux

2: potassium hydroxide / water / 12 h / Sonication

With triethylamine; potassium hydroxide; In dichloromethane; water;
DOI:10.1039/c4ob00865k