(S)-2- ((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(2-(p-tolyl)-1H-indol-3-yl)propanoic acid

Base Information

Chemical Name:(S)-2- ((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(2-(p-tolyl)-1H-indol-3-yl)propanoic acid
CAS No.:1268831-55-5
Molecular Formula:C₃₃H₂₈N₂O₄
Molecular Weight:516.596
Hs Code.:

Synonyms:(S)-2- ((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(2-(p-tolyl)-1H-indol-3-yl)propanoic acid

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Chemical Property of (S)-2- ((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(2-(p-tolyl)-1H-indol-3-yl)propanoic acid

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Technology Process of (S)-2- ((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(2-(p-tolyl)-1H-indol-3-yl)propanoic acid

There total 8 articles about (S)-2- ((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(2-(p-tolyl)-1H-indol-3-yl)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 123726-16-9
bis(4-methylphenyl)iodonium trifluoromethanesulfonate

: 35737-15-6
Fmoc-Trp-OH

: 1268831-55-5
(S)-2- ((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(2-(p-tolyl)-1H-indol-3-yl)propanoic acid

Guidance literature:: With palladium(II) trifluoroacetate; In 1,2-dichloro-ethane; at 70 ℃; for 2h; Reagent/catalyst; Solvent; Temperature; chemoselective reaction; Catalytic behavior;
DOI:10.3184/174751918X15232701502261

Reference yield: 81.0%

: 624-31-7
4-tolyl iodide

: 35737-15-6
Fmoc-Trp-OH

: 1268831-55-5
(S)-2- ((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(2-(p-tolyl)-1H-indol-3-yl)propanoic acid

Guidance literature:: With silver tetrafluoroborate; palladium diacetate; trifluoroacetic acid; In N,N-dimethyl-formamide; at 90 ℃; for 0.333333h; Inert atmosphere; Microwave irradiation; Sealed tube;
DOI:10.1021/jo400961x

Reference yield: 80.0%

: C₂₂H₃₀I⁽¹⁺⁾*CF₃O₃S^(1-)

: 35737-15-6
Fmoc-Trp-OH

: 1268831-55-5
(S)-2- ((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-(2-(p-tolyl)-1H-indol-3-yl)propanoic acid

Guidance literature:: With palladium(II) trifluoroacetate; In 1,2-dichloro-ethane; at 70 ℃; for 2h; chemoselective reaction;
DOI:10.3184/174751918X15232701502261