Benzenamine, 2-(1-methylethyl)-N-2-propenyl- (9CI)

Base Information

• Chemical Name: Benzenamine, 2-(1-methylethyl)-N-2-propenyl- (9CI)
• CAS No.: 368891-61-6
• Molecular Formula: C₁₂H₁₇N
• Molecular Weight: 175.274
• Mol file: 368891-61-6.mol

Synonyms:N-allyl-2-isopropylaniline

Chemical Property of Benzenamine, 2-(1-methylethyl)-N-2-propenyl- (9CI)

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

N-(prop-2-en-1-yl)-2-(propan-2-yl)aniline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzenamine, 2-(1-methylethyl)-N-2-propenyl- (9CI)

There total 1 articles about Benzenamine, 2-(1-methylethyl)-N-2-propenyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

allyl bromide (106-95-6) + 2-isopropylaniline (643-28-7) → N-allyl-2-isopropylaniline (368891-61-6)

Guidance literature:

With sodium carbonate; In chloroform; at 80 ℃; for 10h;

DOI:10.1021/ja003850n

Reference yield: 90.0%

1,2-dichloro-benzene (95-50-1) + N-allyl-2-isopropylaniline (368891-61-6) → 1-(2-isopropylphenyl)-3-methyl-1H-indole

Guidance literature:

With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; sodium t-butanolate; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride; In 1,3,5-trimethyl-benzene; at 80 ℃; for 24h; regioselective reaction; Schlenk technique; Inert atmosphere;

DOI:10.1021/acs.orglett.0c02909

Reference yield: 68.0%

N-allyl-2-isopropylaniline (368891-61-6) → 2-(prop-2-en-1-yl)-6-(propan-2-yl)aniline (368891-62-7)

Guidance literature:

With zinc(II) chloride; In xylene; for 6h; Heating;

DOI:10.1021/ja003850n

upstream raw materials:

allyl bromide

2-isopropylaniline

Downstream raw materials:

2-(prop-2-en-1-yl)-6-(propan-2-yl)aniline

2-isopropyl-6-n-propylaniline