<3-cyano-6-(4-hydrazinocarbonylmethoxyphenyl)-4-phenyl-2-pyridylthio>acethydrazide

Base Information

Chemical Name:<3-cyano-6-(4-hydrazinocarbonylmethoxyphenyl)-4-phenyl-2-pyridylthio>acethydrazide
CAS No.:157223-08-0
Molecular Formula:C₂₂H₂₀N₆O₃S
Molecular Weight:448.505
Hs Code.:

Synonyms:<3-cyano-6-(4-hydrazinocarbonylmethoxyphenyl)-4-phenyl-2-pyridylthio>acethydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <3-cyano-6-(4-hydrazinocarbonylmethoxyphenyl)-4-phenyl-2-pyridylthio>acethydrazide

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Technology Process of <3-cyano-6-(4-hydrazinocarbonylmethoxyphenyl)-4-phenyl-2-pyridylthio>acethydrazide

There total 4 articles about <3-cyano-6-(4-hydrazinocarbonylmethoxyphenyl)-4-phenyl-2-pyridylthio>acethydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 157223-07-9
3-cyano-2-ethoxycarbonylmethylthio-6-(4-ethoxycarbonylmethoxyphenyl)-4-phenylpyridine

: 157223-08-0
<3-cyano-6-(4-hydrazinocarbonylmethoxyphenyl)-4-phenyl-2-pyridylthio>acethydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; for 5h; Heating;
DOI:10.1135/cccc19940978

Reference yield:

: 2657-25-2
(E)-1-(4-hydroxyphenyl)-3-phenylprop-2-en-1-one

: 157223-08-0
<3-cyano-6-(4-hydrazinocarbonylmethoxyphenyl)-4-phenyl-2-pyridylthio>acethydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / Na / methanol / 48 h / 50 °C

2: 89 percent / sodium acetate / ethanol / 3 h / Heating

3: 83 percent / K₂CO₃ / acetone / 21 h / Ambient temperature

4: 77 percent / hydrazine hydrate / ethanol / 5 h / Heating

With sodium acetate; sodium; potassium carbonate; hydrazine hydrate; In methanol; ethanol; acetone;
DOI:10.1135/cccc19940978

Reference yield:

: 157222-84-9
3-cyano-6-(4-hydroxyphenyl)-2-mercapto-4-phenylpyridine

: 157223-08-0
<3-cyano-6-(4-hydrazinocarbonylmethoxyphenyl)-4-phenyl-2-pyridylthio>acethydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / sodium acetate / ethanol / 3 h / Heating

2: 83 percent / K₂CO₃ / acetone / 21 h / Ambient temperature

3: 77 percent / hydrazine hydrate / ethanol / 5 h / Heating

With sodium acetate; potassium carbonate; hydrazine hydrate; In ethanol; acetone;
DOI:10.1135/cccc19940978