3-cyano-2-ethoxycarbonylmethylthio-6-(4-ethoxycarbonylmethoxyphenyl)-4-phenylpyridine

Base Information

Chemical Name:3-cyano-2-ethoxycarbonylmethylthio-6-(4-ethoxycarbonylmethoxyphenyl)-4-phenylpyridine
CAS No.:157223-07-9
Molecular Formula:C₂₆H₂₄N₂O₅S
Molecular Weight:476.553
Hs Code.:

Synonyms:3-cyano-2-ethoxycarbonylmethylthio-6-(4-ethoxycarbonylmethoxyphenyl)-4-phenylpyridine

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Chemical Property of 3-cyano-2-ethoxycarbonylmethylthio-6-(4-ethoxycarbonylmethoxyphenyl)-4-phenylpyridine

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Technology Process of 3-cyano-2-ethoxycarbonylmethylthio-6-(4-ethoxycarbonylmethoxyphenyl)-4-phenylpyridine

There total 4 articles about 3-cyano-2-ethoxycarbonylmethylthio-6-(4-ethoxycarbonylmethoxyphenyl)-4-phenylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 105-39-5
chloroacetic acid ethyl ester

: 157222-84-9
3-cyano-6-(4-hydroxyphenyl)-2-mercapto-4-phenylpyridine

: 157223-07-9
3-cyano-2-ethoxycarbonylmethylthio-6-(4-ethoxycarbonylmethoxyphenyl)-4-phenylpyridine

Guidance literature:: With potassium carbonate; In acetone; for 21h; Heating;
DOI:10.1135/cccc19940978

Reference yield: 83.0%

: 105-39-5
chloroacetic acid ethyl ester

: 157222-94-1
ethyl <3-cyano-6-(4-hydroxyphenyl)-4-phenyl-2-pyridylthio>acetate

: 157223-07-9
3-cyano-2-ethoxycarbonylmethylthio-6-(4-ethoxycarbonylmethoxyphenyl)-4-phenylpyridine

Guidance literature:: With potassium carbonate; In acetone; for 21h; Ambient temperature;
DOI:10.1135/cccc19940978

Reference yield:

: 2657-25-2
(E)-1-(4-hydroxyphenyl)-3-phenylprop-2-en-1-one

: 157223-07-9
3-cyano-2-ethoxycarbonylmethylthio-6-(4-ethoxycarbonylmethoxyphenyl)-4-phenylpyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / Na / methanol / 48 h / 50 °C

2: 89 percent / sodium acetate / ethanol / 3 h / Heating

3: 83 percent / K₂CO₃ / acetone / 21 h / Ambient temperature

With sodium acetate; sodium; potassium carbonate; In methanol; ethanol; acetone;
DOI:10.1135/cccc19940978