N,N'-bis(2-hydroxyethyl)-2-(2-(4-hydroxyphenyl)ethylamino)-1,4,5,8-tetracarboxylic acid 1,8:4,5-diimide

Base Information

Chemical Name:N,N'-bis(2-hydroxyethyl)-2-(2-(4-hydroxyphenyl)ethylamino)-1,4,5,8-tetracarboxylic acid 1,8:4,5-diimide
CAS No.:1421037-07-1
Molecular Formula:C₂₆H₂₃N₃O₇
Molecular Weight:489.485
Hs Code.:

Synonyms:N,N'-bis(2-hydroxyethyl)-2-(2-(4-hydroxyphenyl)ethylamino)-1,4,5,8-tetracarboxylic acid 1,8:4,5-diimide

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Chemical Property of N,N'-bis(2-hydroxyethyl)-2-(2-(4-hydroxyphenyl)ethylamino)-1,4,5,8-tetracarboxylic acid 1,8:4,5-diimide

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Technology Process of N,N'-bis(2-hydroxyethyl)-2-(2-(4-hydroxyphenyl)ethylamino)-1,4,5,8-tetracarboxylic acid 1,8:4,5-diimide

There total 2 articles about N,N'-bis(2-hydroxyethyl)-2-(2-(4-hydroxyphenyl)ethylamino)-1,4,5,8-tetracarboxylic acid 1,8:4,5-diimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 51-67-2
tyrosamine

: 1421037-02-6
N,N'-bis(2-hydroxyethyl)-2,6-dibromonaphthalene-1,4,5,8-tetracarboxylic acid 1,8:4,5-diimide

: 1421037-07-1
N,N'-bis(2-hydroxyethyl)-2-(2-(4-hydroxyphenyl)ethylamino)-1,4,5,8-tetracarboxylic acid 1,8:4,5-diimide

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 8h; Inert atmosphere;
DOI:10.1002/chem.201203097

Reference yield:

: 83204-68-6
2,6-dibromo-1,4,5,8-naphthalenetetracarboxylic acid dianhydride

: 1421037-07-1
N,N'-bis(2-hydroxyethyl)-2-(2-(4-hydroxyphenyl)ethylamino)-1,4,5,8-tetracarboxylic acid 1,8:4,5-diimide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 0.5 h / 130 °C

2: N,N-dimethyl-formamide / 8 h / 20 °C / Inert atmosphere

With acetic acid; In N,N-dimethyl-formamide;
DOI:10.1002/chem.201203097

Reference yield:

: 1421037-07-1
N,N'-bis(2-hydroxyethyl)-2-(2-(4-hydroxyphenyl)ethylamino)-1,4,5,8-tetracarboxylic acid 1,8:4,5-diimide

: 1421037-18-4
N,N'-bis(2-hydroxyethyl)-2-(2-(3-(trimethylamino)methyl-4-hydroxyphenyl)ethylamino)-1,4,5,8-naphthalenetetracarboxylic acid 1,8:4,5-diimide iodide

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethanol / 2 h / Reflux; Inert atmosphere

2.1: sodium hydrogencarbonate / dichloromethane

2.2: 12 h / 20 °C / Inert atmosphere

With sodium hydrogencarbonate; In ethanol; dichloromethane;
DOI:10.1002/chem.201203097