di-tert-butyl (5-{4-[(2,4-dimethoxybenzyl)(1,2,4-thiadiazol-5-yl)sulfamoyl]-2,5-difluorophenoxy}-1,2-benzoxazol-3-yl)imidodicarbonate

Base Information

Chemical Name:di-tert-butyl (5-{4-[(2,4-dimethoxybenzyl)(1,2,4-thiadiazol-5-yl)sulfamoyl]-2,5-difluorophenoxy}-1,2-benzoxazol-3-yl)imidodicarbonate
CAS No.:1432912-84-9
Molecular Formula:C₃₄H₃₅F₂N₅O₁₀S₂
Molecular Weight:775.808
Hs Code.:

Synonyms:di-tert-butyl (5-{4-[(2,4-dimethoxybenzyl)(1,2,4-thiadiazol-5-yl)sulfamoyl]-2,5-difluorophenoxy}-1,2-benzoxazol-3-yl)imidodicarbonate

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Chemical Property of di-tert-butyl (5-{4-[(2,4-dimethoxybenzyl)(1,2,4-thiadiazol-5-yl)sulfamoyl]-2,5-difluorophenoxy}-1,2-benzoxazol-3-yl)imidodicarbonate

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Technology Process of di-tert-butyl (5-{4-[(2,4-dimethoxybenzyl)(1,2,4-thiadiazol-5-yl)sulfamoyl]-2,5-difluorophenoxy}-1,2-benzoxazol-3-yl)imidodicarbonate

There total 5 articles about di-tert-butyl (5-{4-[(2,4-dimethoxybenzyl)(1,2,4-thiadiazol-5-yl)sulfamoyl]-2,5-difluorophenoxy}-1,2-benzoxazol-3-yl)imidodicarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1235406-89-9
N-[(2,4-dimethoxyphenyl)methyl]-2,4,5-trifluoro-N-(1,2,4-thiadiazol-5-yl)benzene-1-sulfonamide

: 1432912-83-8
di-tert-butyl (5-hydroxy-1,2-benzoxazol-3-yl)imidodicarbonate

: 1432912-84-9
di-tert-butyl (5-{4-[(2,4-dimethoxybenzyl)(1,2,4-thiadiazol-5-yl)sulfamoyl]-2,5-difluorophenoxy}-1,2-benzoxazol-3-yl)imidodicarbonate

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; at 20 ℃; for 18h;

Reference yield:

: 34619-03-9
tert-butyldicarbonate

: 1432912-84-9
di-tert-butyl (5-{4-[(2,4-dimethoxybenzyl)(1,2,4-thiadiazol-5-yl)sulfamoyl]-2,5-difluorophenoxy}-1,2-benzoxazol-3-yl)imidodicarbonate

Guidance literature:: Multi-step reaction with 4 steps

1: dmap / tetrahydrofuran / 18 h / 20 °C

2: potassium acetate; bis(triphenylphosphine)palladium(II) dichloride / 1,4-dioxane / 5 h / Reflux; Inert atmosphere

3: dihydrogen peroxide / tetrahydrofuran / 18 h / 20 °C

4: potassium carbonate / dimethyl sulfoxide / 18 h / 20 °C

With dmap; bis(triphenylphosphine)palladium(II) dichloride; dihydrogen peroxide; potassium acetate; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; dimethyl sulfoxide;

Reference yield:

: 455280-00-9
5-bromobenzo[d]isoxazol-3-amine

: 1432912-84-9
di-tert-butyl (5-{4-[(2,4-dimethoxybenzyl)(1,2,4-thiadiazol-5-yl)sulfamoyl]-2,5-difluorophenoxy}-1,2-benzoxazol-3-yl)imidodicarbonate

Guidance literature:: Multi-step reaction with 4 steps

1: dmap / tetrahydrofuran / 18 h / 20 °C

2: potassium acetate; bis(triphenylphosphine)palladium(II) dichloride / 1,4-dioxane / 5 h / Reflux; Inert atmosphere

3: dihydrogen peroxide / tetrahydrofuran / 18 h / 20 °C

4: potassium carbonate / dimethyl sulfoxide / 18 h / 20 °C

With dmap; bis(triphenylphosphine)palladium(II) dichloride; dihydrogen peroxide; potassium acetate; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; dimethyl sulfoxide;