(4,5-diazido-3-benzyloxy-6-p-tolylsulfanyl-tetrahydro-pyran-2-yl)-methanol

Base Information

Chemical Name:(4,5-diazido-3-benzyloxy-6-p-tolylsulfanyl-tetrahydro-pyran-2-yl)-methanol
CAS No.:905704-12-3
Molecular Formula:C₂₀H₂₂N₆O₃S
Molecular Weight:426.499
Hs Code.:

(4,5-diazido-3-benzyloxy-6-<i>p</i>-tolylsulfanyl-tetrahydro-pyran-2-yl)-methanol

Synonyms:(4,5-diazido-3-benzyloxy-6-p-tolylsulfanyl-tetrahydro-pyran-2-yl)-methanol

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Chemical Property of (4,5-diazido-3-benzyloxy-6-p-tolylsulfanyl-tetrahydro-pyran-2-yl)-methanol

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Technology Process of (4,5-diazido-3-benzyloxy-6-p-tolylsulfanyl-tetrahydro-pyran-2-yl)-methanol

There total 1 articles about (4,5-diazido-3-benzyloxy-6-p-tolylsulfanyl-tetrahydro-pyran-2-yl)-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 881895-13-2
p-methylphenyl 2,3-dideoxy-2,3-diazido-1-thio-β-D-mannopyranoside

: 100-39-0
benzyl bromide

: 881895-14-3
(2S,3S,4R,5S,6R)-3,4-Diazido-5-benzyloxy-6-benzyloxymethyl-2-p-tolylsulfanyl-tetrahydro-pyran

: 905704-12-3
(4,5-diazido-3-benzyloxy-6-p-tolylsulfanyl-tetrahydro-pyran-2-yl)-methanol

: 4,5-diazido-2-benzyloxymethyl-6-p-tolylsulfanyl-tetrahydro-pyran-3-ol

Guidance literature:: p-methylphenyl 2,3-dideoxy-2,3-diazido-1-thio-β-D-mannopyranoside; With sodium hydride; In N,N-dimethyl-formamide; at -15 ℃; for 0.0833333h;

benzyl bromide; In N,N-dimethyl-formamide; at -15 - 20 ℃; for 0.5h;
DOI:10.1055/s-2006-939681

Reference yield:

: 905704-12-3
(4,5-diazido-3-benzyloxy-6-p-tolylsulfanyl-tetrahydro-pyran-2-yl)-methanol

: C₂₀H₂₄N₄O₃S

: C₂₀H₂₄N₄O₃S

Guidance literature:: (4,5-diazido-3-benzyloxy-6-p-tolylsulfanyl-tetrahydro-pyran-2-yl)-methanol; With triphenylphosphine; In tetrahydrofuran; at 65 ℃;

With water; In tetrahydrofuran; Further stages. Title compound not separated from byproducts.;
DOI:10.1055/s-2006-950430

Reference yield:

: 905704-12-3
(4,5-diazido-3-benzyloxy-6-p-tolylsulfanyl-tetrahydro-pyran-2-yl)-methanol

: C₃₈H₃₇N₄O₃PS

: C₃₈H₃₇N₄O₃PS

Guidance literature:: With triphenylphosphine; In tetrahydrofuran; at 65 ℃; Title compound not separated from byproducts.;
DOI:10.1055/s-2006-950430