1,1,1-triphenyl-14,17,20,23-tetraoxa-2-thiapentacosan-25-yl methanesulphonate

Base Information

Chemical Name:1,1,1-triphenyl-14,17,20,23-tetraoxa-2-thiapentacosan-25-yl methanesulphonate
CAS No.:1114268-16-4
Molecular Formula:C₃₉H₅₆O₇S₂
Molecular Weight:701.001
Hs Code.:

Synonyms:1,1,1-triphenyl-14,17,20,23-tetraoxa-2-thiapentacosan-25-yl methanesulphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1,1-triphenyl-14,17,20,23-tetraoxa-2-thiapentacosan-25-yl methanesulphonate

Chemical Property:

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Technology Process of 1,1,1-triphenyl-14,17,20,23-tetraoxa-2-thiapentacosan-25-yl methanesulphonate

There total 5 articles about 1,1,1-triphenyl-14,17,20,23-tetraoxa-2-thiapentacosan-25-yl methanesulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1036278-65-5
1,1,1-triphenyl-14,17,20,23-tetraoxa-2-thiapentacosan-25-ol

: 124-63-0
methanesulfonyl chloride

: 1114268-16-4
1,1,1-triphenyl-14,17,20,23-tetraoxa-2-thiapentacosan-25-yl methanesulphonate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja310929s

Reference yield:

: 1611-56-9
1-Bromo-11-hydroxyundecane

: 1114268-16-4
1,1,1-triphenyl-14,17,20,23-tetraoxa-2-thiapentacosan-25-yl methanesulphonate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / ethanol; benzene; water / 20 °C

2: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

3: sodium hydroxide / water / 1 h / 90 °C

4: triethylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

With triethylamine; sodium hydroxide; In ethanol; dichloromethane; water; benzene;
DOI:10.1021/ja310929s

Reference yield:

: 3695-77-0
triphenylmethanethiol

: 1114268-16-4
1,1,1-triphenyl-14,17,20,23-tetraoxa-2-thiapentacosan-25-yl methanesulphonate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydroxide / ethanol; benzene; water / 20 °C

2: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

3: sodium hydroxide / water / 1 h / 90 °C

4: triethylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

With triethylamine; sodium hydroxide; In ethanol; dichloromethane; water; benzene;
DOI:10.1021/ja310929s