C₂₉H₂₈O₅

Base Information

• Chemical Name: C₂₉H₂₈O₅
• CAS No.: 1315279-91-4
• Molecular Formula: C₂₉H₂₈O₅
• Molecular Weight: 456.538
• Mol file: 1315279-91-4.mol

Synonyms:C₂₉H₂₈O₅

Chemical Property of C₂₉H₂₈O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₂₈O₅

There total 4 articles about C₂₉H₂₈O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C30H27F3O7S → C29H28O5 (1315279-91-4)

Guidance literature:

With quaternary nitrite salt QNO₂; In N,N-dimethyl-formamide; at 50 ℃; for 16h; Inert atmosphere;

DOI:10.1016/j.bmc.2011.05.007

Reference yield:

2-naphthyl 2,4-di-O-benzyl-β-D-xylopyranoside (1315279-66-3) → C29H28O5 (1315279-91-4)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 2 h / -10 °C / Inert atmosphere

2: quaternary nitrite salt QNO₂ / N,N-dimethyl-formamide / 16 h / 50 °C / Inert atmosphere

With pyridine; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/j.bmc.2011.05.007

Reference yield:

benzyl bromide (100-39-0) → C29H28O5 (1315279-91-4)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium hydroxide / dichloromethane / 22 h / 20 °C

2: pyridine / dichloromethane / 2 h / -10 °C / Inert atmosphere

3: quaternary nitrite salt QNO₂ / N,N-dimethyl-formamide / 16 h / 50 °C / Inert atmosphere

With pyridine; potassium hydroxide; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/j.bmc.2011.05.007

upstream raw materials:

2-naphthyl 2,4-di-O-benzyl-β-D-xylopyranoside

benzyl bromide

Downstream raw materials:

2-naphthyl 2,4-di-O-benzyl-3-deoxy-3-fluoro-β-D-xylopyranoside