1-O-(4'-methoxybenzyl)-2,3,4,6-tetra-O-benzyl-myo-inositol-5-(dibenzyl phosphate)

Base Information

Chemical Name:1-O-(4'-methoxybenzyl)-2,3,4,6-tetra-O-benzyl-myo-inositol-5-(dibenzyl phosphate)
CAS No.:291527-84-9
Molecular Formula:C₅₆H₅₇O₁₀P
Molecular Weight:921.036
Hs Code.:

Synonyms:1-O-(4'-methoxybenzyl)-2,3,4,6-tetra-O-benzyl-myo-inositol-5-(dibenzyl phosphate)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-O-(4'-methoxybenzyl)-2,3,4,6-tetra-O-benzyl-myo-inositol-5-(dibenzyl phosphate)

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Technology Process of 1-O-(4'-methoxybenzyl)-2,3,4,6-tetra-O-benzyl-myo-inositol-5-(dibenzyl phosphate)

There total 6 articles about 1-O-(4'-methoxybenzyl)-2,3,4,6-tetra-O-benzyl-myo-inositol-5-(dibenzyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 81927-55-1
O-benzyl 2,2,2-trichloroacetimidate

: 291527-89-4
Phosphoric acid dibenzyl ester (1S,2R,3S,4R,5R,6S)-2,6-bis-benzyloxy-3,4-dihydroxy-5-(4-methoxy-benzyloxy)-cyclohexyl ester

: 291527-84-9
1-O-(4'-methoxybenzyl)-2,3,4,6-tetra-O-benzyl-myo-inositol-5-(dibenzyl phosphate)

Guidance literature:: With trityl tetrafluoroborate; In diethyl ether; at 23 ℃; for 36h;
DOI:10.1016/S0040-4039(00)00465-2

Reference yield:

: C₅₆H₅₇O₉P

: 291527-84-9
1-O-(4'-methoxybenzyl)-2,3,4,6-tetra-O-benzyl-myo-inositol-5-(dibenzyl phosphate)

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 - 20 ℃; for 3.5h; Inert atmosphere;
DOI:10.1039/b913399b

Reference yield:

: 98510-25-9
meso-4,6-di-O-benzyl-D-myo-inositol-1,3,5-O-orthoformate

: 291527-84-9
1-O-(4'-methoxybenzyl)-2,3,4,6-tetra-O-benzyl-myo-inositol-5-(dibenzyl phosphate)

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / 10 N HCl / methanol / 0.45 h / 65 °C

2: PTSA / CH₂Cl₂ / 4 h / 23 °C

4: 77 percent / CF₃CO₂H / CH₂Cl₂; methanol / 0.5 h / 0 °C

5: 73 percent / Ph₃CBF₄ / diethyl ether / 36 h / 23 °C

With hydrogenchloride; trityl tetrafluoroborate; toluene-4-sulfonic acid; trifluoroacetic acid; In methanol; diethyl ether; dichloromethane; 1: Hydrolysis / 2: Condensation / 4: Substitution / 5: Alkylation;
DOI:10.1016/S0040-4039(00)00465-2