di-cyclohexyl selenide

Base Information

• Chemical Name: di-cyclohexyl selenide
• CAS No.: 56592-92-8
• Molecular Formula: C₁₂H₂₂Se
• Molecular Weight: 245.267
• Mol file: 56592-92-8.mol

Synonyms:di-cyclohexyl selenide

Chemical Property of di-cyclohexyl selenide

Chemical Property:

Purity/Quality:

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Technology Process of di-cyclohexyl selenide

There total 6 articles about di-cyclohexyl selenide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

1-bromocyclohexane (108-85-0) → di-cyclohexyl selenide (56592-92-8)

Guidance literature:

With selenium; magnesium; In tetrahydrofuran; toluene; at 86 ℃; for 12h; Inert atmosphere;

DOI:10.3998/ark.5550190.0013.814

Reference yield: 18.0%

cyclohexyl chloride (542-18-7) → di-cyclohexyl selenide (56592-92-8) + 1,2-dicyclohexyl diselenide (56592-97-3)

Guidance literature:

With O₂S₂Se^(2-)*2Na⁽¹⁺⁾; In ethanol; water; at 100 ℃; for 48h; Sealed tube;

DOI:10.1055/s-0037-1612083

Reference yield:

Cyclohexanecarboxylic acid (98-89-5) → di-cyclohexyl selenide (56592-92-8)

Guidance literature:

With selenium; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 150 ℃; for 20h; Inert atmosphere;

DOI:10.1002/aoc.4599

upstream raw materials:

cyclohexene

1-bromocyclohexane

Cyclohexanecarboxylic acid

cyclohexyl chloride