[2-((S)-2-Amino-4-methanesulfinyl-butyldisulfanylmethyl)-3-phenyl-propionylamino]-acetic acid benzyl ester

Base Information

Chemical Name:[2-((S)-2-Amino-4-methanesulfinyl-butyldisulfanylmethyl)-3-phenyl-propionylamino]-acetic acid benzyl ester
CAS No.:135949-61-0
Molecular Formula:C₂₄H₃₂N₂O₄S₃
Molecular Weight:508.727
Hs Code.:

Synonyms:[2-((S)-2-Amino-4-methanesulfinyl-butyldisulfanylmethyl)-3-phenyl-propionylamino]-acetic acid benzyl ester

Suppliers and Price of [2-((S)-2-Amino-4-methanesulfinyl-butyldisulfanylmethyl)-3-phenyl-propionylamino]-acetic acid benzyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [2-((S)-2-Amino-4-methanesulfinyl-butyldisulfanylmethyl)-3-phenyl-propionylamino]-acetic acid benzyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [2-((S)-2-Amino-4-methanesulfinyl-butyldisulfanylmethyl)-3-phenyl-propionylamino]-acetic acid benzyl ester

There total 8 articles about [2-((S)-2-Amino-4-methanesulfinyl-butyldisulfanylmethyl)-3-phenyl-propionylamino]-acetic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 141437-99-2
[2-((S)-2-tert-Butoxycarbonylamino-4-methanesulfinyl-butyldisulfanylmethyl)-3-phenyl-propionylamino]-acetic acid benzyl ester

: 135949-61-0
[2-((S)-2-Amino-4-methanesulfinyl-butyldisulfanylmethyl)-3-phenyl-propionylamino]-acetic acid benzyl ester

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.1021/jm00091a016

Reference yield:

: 141437-94-7
((S)-1-Mercaptomethyl-3-methylsulfanyl-propyl)-carbamic acid tert-butyl ester

: 135949-61-0
[2-((S)-2-Amino-4-methanesulfinyl-butyldisulfanylmethyl)-3-phenyl-propionylamino]-acetic acid benzyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / CH₃COOH / ethanol / Ambient temperature

2: 64 percent / ethanol / Ambient temperature

3: 70 percent / 0.2 M aq. NaIO₄ / ethanol / 0 °C

4: 78 percent / CF₃COOH / CH₂Cl₂ / 3 h / 0 - 20 °C

With sodium periodate; acetic acid; trifluoroacetic acid; In ethanol; dichloromethane;
DOI:10.1021/jm00091a016

Reference yield:

: 139429-04-2
Thioacetic acid S-((S)-2-tert-butoxycarbonylamino-4-methylsulfanyl-butyl) ester

: 135949-61-0
[2-((S)-2-Amino-4-methanesulfinyl-butyldisulfanylmethyl)-3-phenyl-propionylamino]-acetic acid benzyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / 1 M NaOH / ethanol / 3 h / 0 - 20 °C

2: 75 percent / CH₃COOH / ethanol / Ambient temperature

3: 64 percent / ethanol / Ambient temperature

4: 70 percent / 0.2 M aq. NaIO₄ / ethanol / 0 °C

5: 78 percent / CF₃COOH / CH₂Cl₂ / 3 h / 0 - 20 °C

With sodium hydroxide; sodium periodate; acetic acid; trifluoroacetic acid; In ethanol; dichloromethane;
DOI:10.1021/jm00091a016