C₁₄H₁₆Br₂N₂

Base Information

• Chemical Name: C₁₄H₁₆Br₂N₂
• CAS No.: 1246624-44-1
• Molecular Formula: C₁₄H₁₆Br₂N₂
• Molecular Weight: 372.102
• Mol file: 1246624-44-1.mol

Synonyms:C₁₄H₁₆Br₂N₂

Chemical Property of C₁₄H₁₆Br₂N₂

Chemical Property:

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Technology Process of C₁₄H₁₆Br₂N₂

There total 1 articles about C₁₄H₁₆Br₂N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

N-methyl-2,4,5-tribromoimidazole (1003-91-4) + p-tert-butylphenylboronic acid (123324-71-0) → C14H16Br2N2 (1246624-44-1)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,4-dioxane; water; toluene; at 100 ℃; for 12h;

DOI:10.1055/s-0030-1258092

Reference yield: 81.0%

C14H16Br2N2 (1246624-44-1) + ethyl acrylate (140-88-5,9003-32-1) → C24H30N2O4

Guidance literature:

With palladium diacetate; triethylamine; tricyclohexylphosphine; In N,N-dimethyl-formamide; at 100 ℃; for 24h; Inert atmosphere; pressure tube;

DOI:10.1055/s-0030-1258092

Reference yield: 64.0%

4-Methoxystyrene (637-69-4,24936-44-5) + C14H16Br2N2 (1246624-44-1) → C32H34N2O2

Guidance literature:

With palladium diacetate; triethylamine; tricyclohexylphosphine; In N,N-dimethyl-formamide; at 100 ℃; for 24h; Inert atmosphere; pressure tube;

DOI:10.1055/s-0030-1258092

upstream raw materials:

N-methyl-2,4,5-tribromoimidazole

p-tert-butylphenylboronic acid

Refernces