N-[(S)-1-phenylethyl]-2-(5-benzyloxy-2-bromo-4-methoxyphenyl)ethylamine

Base Information

Chemical Name:N-[(S)-1-phenylethyl]-2-(5-benzyloxy-2-bromo-4-methoxyphenyl)ethylamine
CAS No.:342901-82-0
Molecular Formula:C₂₄H₂₆BrNO₂
Molecular Weight:440.38
Hs Code.:

Synonyms:N-[(S)-1-phenylethyl]-2-(5-benzyloxy-2-bromo-4-methoxyphenyl)ethylamine

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Chemical Property of N-[(S)-1-phenylethyl]-2-(5-benzyloxy-2-bromo-4-methoxyphenyl)ethylamine

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Technology Process of N-[(S)-1-phenylethyl]-2-(5-benzyloxy-2-bromo-4-methoxyphenyl)ethylamine

There total 2 articles about N-[(S)-1-phenylethyl]-2-(5-benzyloxy-2-bromo-4-methoxyphenyl)ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13425-04-2
5-benzyloxy-4-methoxy-2-bromophenylacetic acid

: 342901-82-0
N-[(S)-1-phenylethyl]-2-(5-benzyloxy-2-bromo-4-methoxyphenyl)ethylamine

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂

2: 96.7 percent / Na₂CO₃ / diethyl ether / 2 h / 10 - 15 °C

3: 92.4 percent / BF₃*Et₂O; BH₃*THF / tetrahydrofuran / 2.5 h / 70 °C

With thionyl chloride; borane-THF; boron trifluoride diethyl etherate; sodium carbonate; In tetrahydrofuran; diethyl ether;
DOI:10.3987/com-00-9151

Reference yield:

: 86639-19-2
5-benzyloxy-2-bromo-4-methoxyphenylacetic acid chloride

: 342901-82-0
N-[(S)-1-phenylethyl]-2-(5-benzyloxy-2-bromo-4-methoxyphenyl)ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 96.7 percent / Na₂CO₃ / diethyl ether / 2 h / 10 - 15 °C

2: 92.4 percent / BF₃*Et₂O; BH₃*THF / tetrahydrofuran / 2.5 h / 70 °C

With borane-THF; boron trifluoride diethyl etherate; sodium carbonate; In tetrahydrofuran; diethyl ether;
DOI:10.3987/com-00-9151