O-ethyl 4-(4-(5-(5-nitrofuran-2-yl)-1,3,4-thiadiazol-2-yl)piperazin-1-yl)benzimidate hydrochloride

Base Information

Chemical Name:O-ethyl 4-(4-(5-(5-nitrofuran-2-yl)-1,3,4-thiadiazol-2-yl)piperazin-1-yl)benzimidate hydrochloride
CAS No.:1310494-14-4
Molecular Formula:C₁₉H₂₀N₆O₄S*ClH
Molecular Weight:464.933
Hs Code.:

Synonyms:O-ethyl 4-(4-(5-(5-nitrofuran-2-yl)-1,3,4-thiadiazol-2-yl)piperazin-1-yl)benzimidate hydrochloride

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Chemical Property of O-ethyl 4-(4-(5-(5-nitrofuran-2-yl)-1,3,4-thiadiazol-2-yl)piperazin-1-yl)benzimidate hydrochloride

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Technology Process of O-ethyl 4-(4-(5-(5-nitrofuran-2-yl)-1,3,4-thiadiazol-2-yl)piperazin-1-yl)benzimidate hydrochloride

There total 6 articles about O-ethyl 4-(4-(5-(5-nitrofuran-2-yl)-1,3,4-thiadiazol-2-yl)piperazin-1-yl)benzimidate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64-17-5
ethanol

: 1310494-13-3
4-(4-(5-(5-nitrofuran-2-yl)-1,3,4-thiadiazol-2-yl)piperazin-1-yl)benzonitrile

: 1310494-14-4
O-ethyl 4-(4-(5-(5-nitrofuran-2-yl)-1,3,4-thiadiazol-2-yl)piperazin-1-yl)benzimidate hydrochloride

Guidance literature:: With hydrogenchloride; In dichloromethane; at 20 ℃; for 120h;
DOI:10.1016/j.ejmech.2011.03.053

Reference yield:

: 1194-02-1,143234-87-1
4-fluorobenzonitrile

: 1310494-14-4
O-ethyl 4-(4-(5-(5-nitrofuran-2-yl)-1,3,4-thiadiazol-2-yl)piperazin-1-yl)benzimidate hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / butanone / 96 h / Reflux

2: potassium carbonate / butanone / 8 h / Reflux

3: hydrogenchloride / dichloromethane / 120 h / 20 °C

With hydrogenchloride; potassium carbonate; In dichloromethane; butanone;
DOI:10.1016/j.ejmech.2011.03.053

Reference yield:

: 4015-11-6
2-chloro-5-(5-nitrofuran-2-yl)-1,3,4-thiadiazole

: 1310494-14-4
O-ethyl 4-(4-(5-(5-nitrofuran-2-yl)-1,3,4-thiadiazol-2-yl)piperazin-1-yl)benzimidate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / butanone / 8 h / Reflux

2: hydrogenchloride / dichloromethane / 120 h / 20 °C

With hydrogenchloride; potassium carbonate; In dichloromethane; butanone;
DOI:10.1016/j.ejmech.2011.03.053