4-bromo-N-cyclohexyl-2-nitroaniline

Base Information

Chemical Name:4-bromo-N-cyclohexyl-2-nitroaniline
CAS No.:87815-76-7
Molecular Formula:C₁₂H₁₅BrN₂O₂
Molecular Weight:299.167
Hs Code.:
DSSTox Substance ID:DTXSID101279714

Synonyms:4-bromo-N-cyclohexyl-2-nitroaniline;87815-76-7;SCHEMBL16538351;GETFCHBWBHFHBW-UHFFFAOYSA-N;DTXSID101279714;AKOS008958415;4-Bromo-N-cyclohexyl-2-nitrobenzenamine

Suppliers and Price of 4-bromo-N-cyclohexyl-2-nitroaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-bromo-N-cyclohexyl-2-nitroaniline

Chemical Property:

XLogP3:4.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:298.03169
Heavy Atom Count:17
Complexity:264

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CCC(CC1)NC2=C(C=C(C=C2)Br)[N+](=O)[O-]

Technology Process of 4-bromo-N-cyclohexyl-2-nitroaniline

There total 3 articles about 4-bromo-N-cyclohexyl-2-nitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 364-73-8
4-Bromo-1-fluoro-2-nitrobenzene

: 108-91-8,157973-60-9
cyclohexylamine

: 87815-76-7
4-bromo-N-cyclohexyl-2-nitroaniline

Guidance literature:: In ethanol; at 20 ℃; for 24h;
DOI:10.1021/jacs.8b08152

Reference yield:

: 106-37-6
1.4-dibromobenzene

: 87815-76-7
4-bromo-N-cyclohexyl-2-nitroaniline

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid; nitric acid / dichloromethane / 0.5 h / 0 °C

2: potassium carbonate / N,N-dimethyl-formamide / 18 h / 100 °C

With sulfuric acid; nitric acid; potassium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c8ob02973c