C₁₅H₂₇NO₅S

Base Information

Chemical Name:C₁₅H₂₇NO₅S
CAS No.:1192424-59-1
Molecular Formula:C₁₅H₂₇NO₅S
Molecular Weight:333.449
Hs Code.:

C<sub>15</sub>H<sub>27</sub>NO<sub>5</sub>S

Synonyms:C₁₅H₂₇NO₅S

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Chemical Property of C₁₅H₂₇NO₅S

Chemical Property:

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Technology Process of C₁₅H₂₇NO₅S

There total 3 articles about C₁₅H₂₇NO₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 342578-12-5
C₁₁H₂₁NO₄S

: 141-78-6
ethyl acetate

: 1192424-59-1
C₁₅H₂₇NO₅S

Guidance literature:: C₁₁H₂₁NO₄S; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 4 - 20 ℃; for 1h;

ethyl acetate; With 1-methyl-1H-imidazole; titanium tetrachloride; In dichloromethane; at -60 ℃; for 0.5h;

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -40 ℃; for 0.666667h;

Reference yield:

: 1195758-84-9
C₁₁H₂₀ClNO₃S

: 141-78-6
ethyl acetate

: 1192424-59-1
C₁₅H₂₇NO₅S

Guidance literature:: C₁₁H₂₀ClNO₃S; ethyl acetate; With 1-methyl-1H-imidazole; titanium tetrachloride; In dichloromethane; at -60 ℃; for 0.5h;

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -40 ℃; for 0.666667h;

Reference yield:

: 342578-12-5
C₁₁H₂₁NO₄S

: 1192424-59-1
C₁₅H₂₇NO₅S

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C

2.1: 1-methyl-1H-imidazole / titanium tetrachloride / dichloromethane / 0.5 h / -60 °C

2.2: 0.67 h / -40 °C

With 1-methyl-1H-imidazole; oxalyl dichloride; titanium tetrachloride; N,N-dimethyl-formamide; In dichloromethane;