ethyl 4-<2-<2-(3-acetylthiazolidin-2-yl)phenylsulfonylamino>ethyl>phenoxyacetate

Base Information

Chemical Name:ethyl 4-<2-<2-(3-acetylthiazolidin-2-yl)phenylsulfonylamino>ethyl>phenoxyacetate
CAS No.:156781-24-7
Molecular Formula:C₂₃H₂₈N₂O₆S₂
Molecular Weight:492.617
Hs Code.:

Synonyms:ethyl 4-<2-<2-(3-acetylthiazolidin-2-yl)phenylsulfonylamino>ethyl>phenoxyacetate

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Chemical Property of ethyl 4-<2-<2-(3-acetylthiazolidin-2-yl)phenylsulfonylamino>ethyl>phenoxyacetate

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Technology Process of ethyl 4-<2-<2-(3-acetylthiazolidin-2-yl)phenylsulfonylamino>ethyl>phenoxyacetate

There total 6 articles about ethyl 4-<2-<2-(3-acetylthiazolidin-2-yl)phenylsulfonylamino>ethyl>phenoxyacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.7%

: 75-36-5
acetyl chloride

: 156781-23-6
ethyl 4-<2-<2-(thiazolidin-2-yl)phenylsulfonylamino>ethyl>phenoxyacetate

: 156781-24-7
ethyl 4-<2-<2-(3-acetylthiazolidin-2-yl)phenylsulfonylamino>ethyl>phenoxyacetate

Guidance literature:: With pyridine; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1248/cpb.42.521

Reference yield:

: 1008-72-6
sodium 2-formylbenzenesulfonate

: 156781-24-7
ethyl 4-<2-<2-(3-acetylthiazolidin-2-yl)phenylsulfonylamino>ethyl>phenoxyacetate

Guidance literature:: Multi-step reaction with 6 steps

1: 35.9 percent / SOCl₂, DMF / 0.05 h / 100 °C

2: 83 percent / conc. H₂SO₄ / 0.5 h

3: 94.6 percent / Et₃N / CH₂Cl₂ / 0.5 h / Ambient temperature

4: 74.7 percent / EtONa / ethanol / 10 h / Ambient temperature

5: 82.4 percent / ethanol / 72 h / Ambient temperature

6: 42.7 percent / pyridine / CH₂Cl₂ / 1 h / Ambient temperature

With pyridine; thionyl chloride; sulfuric acid; sodium ethanolate; triethylamine; N,N-dimethyl-formamide; In ethanol; dichloromethane;
DOI:10.1248/cpb.42.521

Reference yield:

: 156781-20-3
2-(bis-acetoxymethyl)phenylsulfonyl chloride

: 156781-24-7
ethyl 4-<2-<2-(3-acetylthiazolidin-2-yl)phenylsulfonylamino>ethyl>phenoxyacetate

Guidance literature:: Multi-step reaction with 4 steps

1: 94.6 percent / Et₃N / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 74.7 percent / EtONa / ethanol / 10 h / Ambient temperature

3: 82.4 percent / ethanol / 72 h / Ambient temperature

4: 42.7 percent / pyridine / CH₂Cl₂ / 1 h / Ambient temperature

With pyridine; sodium ethanolate; triethylamine; In ethanol; dichloromethane;
DOI:10.1248/cpb.42.521