C₁₄H₂₁NO₄

Base Information

Chemical Name:C₁₄H₂₁NO₄
CAS No.:1354784-99-8
Molecular Formula:C₁₄H₂₁NO₄
Molecular Weight:267.325
Hs Code.:

C<sub>14</sub>H<sub>21</sub>NO<sub>4</sub>

Synonyms:C₁₄H₂₁NO₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₂₁NO₄

Chemical Property:

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Technology Process of C₁₄H₂₁NO₄

There total 3 articles about C₁₄H₂₁NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1354784-86-3
C₁₅H₂₃NO₄

: 1354784-99-8
C₁₄H₂₁NO₄

Guidance literature:: With boron trichloride; In dichloromethane; at 20 ℃; for 0.666667h; regioselective reaction;
DOI:10.1016/j.tetlet.2011.11.062

Reference yield:

: 490-64-2
asaronic acid

: 1354784-99-8
C₁₄H₂₁NO₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: pivaloyl chloride; triethylamine / tetrahydrofuran / 1 h / 0 °C

1.2: 5 h / 0 - 20 °C

2.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / tetrahydrofuran / 0.5 h / -78 °C

2.2: 2 h / -78 - -20 °C

3.1: boron trichloride / dichloromethane / 0.67 h / 20 °C

With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; pivaloyl chloride; boron trichloride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2011.11.062

Reference yield:

: 105518-12-5
N,N-diethyl-2,4,5-trimethoxybenzamide

: 1354784-99-8
C₁₄H₂₁NO₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / tetrahydrofuran / 0.5 h / -78 °C

1.2: 2 h / -78 - -20 °C

2.1: boron trichloride / dichloromethane / 0.67 h / 20 °C

With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; boron trichloride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2011.11.062