5-methyl-4-(2-hydroxyethoxy)-1,2-benzenedicarboxylic acid bis(methyl ester)

Base Information

Chemical Name:5-methyl-4-(2-hydroxyethoxy)-1,2-benzenedicarboxylic acid bis(methyl ester)
CAS No.:116809-94-0
Molecular Formula:C₁₃H₁₆O₆
Molecular Weight:268.266
Hs Code.:

Synonyms:5-methyl-4-(2-hydroxyethoxy)-1,2-benzenedicarboxylic acid bis(methyl ester)

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Chemical Property of 5-methyl-4-(2-hydroxyethoxy)-1,2-benzenedicarboxylic acid bis(methyl ester)

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Technology Process of 5-methyl-4-(2-hydroxyethoxy)-1,2-benzenedicarboxylic acid bis(methyl ester)

There total 1 articles about 5-methyl-4-(2-hydroxyethoxy)-1,2-benzenedicarboxylic acid bis(methyl ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 116809-87-1
3,6-dihydro-5-methyl-3,4-(ethylenedioxy)-1,2-benzenedicarboxylic acid bis(methyl ester)

: 116809-94-0
5-methyl-4-(2-hydroxyethoxy)-1,2-benzenedicarboxylic acid bis(methyl ester)

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; Heating;
DOI:10.1021/jo00259a012

Reference yield: 67.0%

: 116809-94-0
5-methyl-4-(2-hydroxyethoxy)-1,2-benzenedicarboxylic acid bis(methyl ester)

: 116809-99-5
5-methyl-4-(2-bromoethoxy)-1,2-benzenedicarboxylic acid bis(methyl ester)

Guidance literature:: With bromine; triphenylphosphine; In acetonitrile;
DOI:10.1021/jo00259a012

Reference yield:

: 116809-94-0
5-methyl-4-(2-hydroxyethoxy)-1,2-benzenedicarboxylic acid bis(methyl ester)

: 22481-13-6
5-methyl-4-hydroxy-1,2-benzenedicarboxylic acid bis(methyl ester)

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / Br₂, Ph₃P / acetonitrile

2: 88 percent / aq. NH₄Cl, Zn / ethanol / 1 h / Heating

With bromine; ammonium chloride; triphenylphosphine; zinc; In ethanol; acetonitrile;
DOI:10.1021/jo00259a012