2,2'-(1,3,6,8-tetraoxo-1,3,6,8-tetrahydrobenzo[lmn][3,8]phenanthroline-2,7-diyl)bis(3-phenylpropanoic acid)

Base Information

Chemical Name:2,2'-(1,3,6,8-tetraoxo-1,3,6,8-tetrahydrobenzo[lmn][3,8]phenanthroline-2,7-diyl)bis(3-phenylpropanoic acid)
CAS No.:856410-83-8
Molecular Formula:C₃₂H₂₂N₂O₈
Molecular Weight:562.535
Hs Code.:

Synonyms:2,2'-(1,3,6,8-tetraoxo-1,3,6,8-tetrahydrobenzo[lmn][3,8]phenanthroline-2,7-diyl)bis(3-phenylpropanoic acid)

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Chemical Property of 2,2'-(1,3,6,8-tetraoxo-1,3,6,8-tetrahydrobenzo[lmn][3,8]phenanthroline-2,7-diyl)bis(3-phenylpropanoic acid)

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Technology Process of 2,2'-(1,3,6,8-tetraoxo-1,3,6,8-tetrahydrobenzo[lmn][3,8]phenanthroline-2,7-diyl)bis(3-phenylpropanoic acid)

There total 1 articles about 2,2'-(1,3,6,8-tetraoxo-1,3,6,8-tetrahydrobenzo[lmn][3,8]phenanthroline-2,7-diyl)bis(3-phenylpropanoic acid) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 81-30-1
1,4,5,8-naphthalenetetracarboxylic dianhydride

: 856410-83-8
2,2'-(1,3,6,8-tetraoxo-1,3,6,8-tetrahydrobenzo[lmn][3,8]phenanthroline-2,7-diyl)bis(3-phenylpropanoic acid)

Guidance literature:: In N,N-dimethyl-formamide; at 110 ℃; for 16h;
DOI:10.3762/bjoc.9.178

Reference yield: 52.0%

: 856410-83-8
2,2'-(1,3,6,8-tetraoxo-1,3,6,8-tetrahydrobenzo[lmn][3,8]phenanthroline-2,7-diyl)bis(3-phenylpropanoic acid)

: 93324-65-3
1-methylaminopyrene hydrochloride

: C₆₆H₄₄N₄O₆

Guidance literature:: 2,2'-(1,3,6,8-tetraoxo-1,3,6,8-tetrahydrobenzo[lmn][3,8]phenanthroline-2,7-diyl)bis(3-phenylpropanoic acid); With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; for 0.25h; Inert atmosphere; Cooling with ice;

1-methylaminopyrene hydrochloride; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.3762/bjoc.9.178

Reference yield: 50.0%

: 2577-90-4
methyl (2S)-2-amino-3-phenylpropanoate

: 856410-83-8
2,2'-(1,3,6,8-tetraoxo-1,3,6,8-tetrahydrobenzo[lmn][3,8]phenanthroline-2,7-diyl)bis(3-phenylpropanoic acid)

: 1380412-22-5
N,N-bis-(Phe-Phe-OMe) NDI

Guidance literature:: 2,2'-(1,3,6,8-tetraoxo-1,3,6,8-tetrahydrobenzo[lmn][3,8]phenanthroline-2,7-diyl)bis(3-phenylpropanoic acid); With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; for 0.25h;

methyl (2S)-2-amino-3-phenylpropanoate; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1002/chem.201200197