3-(3,4-dihydroxyphenyl)-N-{1-[2-(3,4-dihydroxyphenyl)ethylcarbamoyl]-2-(tritylsulfanyl)ethyl}acrylamide

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Chemical Name:3-(3,4-dihydroxyphenyl)-N-{1-[2-(3,4-dihydroxyphenyl)ethylcarbamoyl]-2-(tritylsulfanyl)ethyl}acrylamide
CAS No.:406727-56-8
Molecular Formula:C₃₉H₃₆N₂O₆S
Molecular Weight:660.791
Hs Code.:

Synonyms:3-(3,4-dihydroxyphenyl)-N-{1-[2-(3,4-dihydroxyphenyl)ethylcarbamoyl]-2-(tritylsulfanyl)ethyl}acrylamide

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Chemical Property of 3-(3,4-dihydroxyphenyl)-N-{1-[2-(3,4-dihydroxyphenyl)ethylcarbamoyl]-2-(tritylsulfanyl)ethyl}acrylamide

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Technology Process of 3-(3,4-dihydroxyphenyl)-N-{1-[2-(3,4-dihydroxyphenyl)ethylcarbamoyl]-2-(tritylsulfanyl)ethyl}acrylamide

There total 5 articles about 3-(3,4-dihydroxyphenyl)-N-{1-[2-(3,4-dihydroxyphenyl)ethylcarbamoyl]-2-(tritylsulfanyl)ethyl}acrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 331-39-5,501-16-6
caffeic acid

: 1370349-51-1
2-amino-N-[2-(3,4-dihydroxyphenyl)ethyl]-3-(tritylsulfanyl)propionamide

: 406727-56-8
3-(3,4-dihydroxyphenyl)-N-{1-[2-(3,4-dihydroxyphenyl)ethylcarbamoyl]-2-(tritylsulfanyl)ethyl}acrylamide

Guidance literature:: With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 12.5h; Inert atmosphere;
DOI:10.1016/j.ejmech.2012.02.018

Reference yield:

: 76-84-6
triphenylmethyl alcohol

: 406727-56-8
3-(3,4-dihydroxyphenyl)-N-{1-[2-(3,4-dihydroxyphenyl)ethylcarbamoyl]-2-(tritylsulfanyl)ethyl}acrylamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: trifluoroacetic acid / 2 h

1.2: 0 °C / pH 5 - 6

2.1: sodium hydroxide / water / 24 h / 20 °C

2.2: pH 2

3.1: dicyclohexyl-carbodiimide / acetonitrile / 14 h / 0 - 20 °C / Inert atmosphere

4.1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C

5.1: trifluoroacetic acid / water / 3 h

6.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 12.5 h / 0 - 20 °C / Inert atmosphere

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; sodium hydroxide; In water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.ejmech.2012.02.018

Reference yield:

: 2799-07-7
S-trityl-L-cysteine

: 406727-56-8
3-(3,4-dihydroxyphenyl)-N-{1-[2-(3,4-dihydroxyphenyl)ethylcarbamoyl]-2-(tritylsulfanyl)ethyl}acrylamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / water / 24 h / 20 °C

1.2: pH 2

2.1: dicyclohexyl-carbodiimide / acetonitrile / 14 h / 0 - 20 °C / Inert atmosphere

3.1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C

4.1: trifluoroacetic acid / water / 3 h

5.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 12.5 h / 0 - 20 °C / Inert atmosphere

With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; sodium hydroxide; In water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.ejmech.2012.02.018